GCMS quantitation results for sample AE10242, May 2002

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Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020516\10242.D Vial: 18 Acq On : 17 May 2002 2:09 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 5 Phenanthrene-diO Concentration Rank 3 R.T. EstConc Area Relative to. ISTD R.T. 31.95 0.35 ug/1 25201 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phen. .threne-dlO 188 C14D10 001517-22-2 53 2 Quin zoline, 4-(1-methylethyl)-,... 188 C11H12N2O 050915-32-7 43 3 Anthracene-d10- 188 C14D10 001719-06-8 42 4 4-p^ethyl-2- (3-fluorophenyl)pyrim. . . 188 C11H9FN2 076128-66-0 25 Abundance Scan 4913 (31.946 min): 10242.D (-4906) (-) m/z 188.20 100.00% 150

5000

66 80 94 160 . 31.60 31.80 32.00 32.20 +FFT ---HHHHH ■p-TTT m/z 79.90 19.38%| m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 its

5000 31,60 31.80 32.00 32.20 80 m/ z 80.20 19.26%I 94 160 30 42 52 66 . TIOmP)MTH 1l108118.—132.146—4179179L— mz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79808: Quinazoline, 4-(1-methylethyl)-, 1-oxide its

173 31.60 31.80 32.00 32.20 5000 m/z 184.10 19.17% 157 77 91 115 131 146

Ti/Z-> +----7+- — -H 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 ■p-n-r

Abundance: #79826: Anthracene-d1 0- its 31.60 31.80 32.00 32.20 m/z 160.20 15.21%| 5000

66 80 94 160 , . / 4 । . । . ।

m/z—> 17 30 42 52 TITTUTTH -Hl108,118,.132.146.44170179—— 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

10242.D SCAN020507.M Fri May 17 10:41:21 2002 Page 7

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