GCMS quantitation results for sample AE10242, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020516\10242.D Vial: 18 Acq On : 17 May 2002 2:09 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 6 2-Trifluoroacetoxytridecane Concentration Rank 5 R.T. EstConc Area Relative to. I STD R.T. 36.44 0.29 ug/1 17730 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Trifluoroacetoxytridecane 296 C15H27F3O2 1000245-47-1 59 2 1-Decanethiol 174 C10H22S 000143-10-2 58 3 1-Tricosene 322 C23H46 018835-32-0 50 4 1-Octadecene 252 C18H36 000112-88-9 50 Abundance Scan 5678 (36.441 min): 10242.D (-5668) (-) m/ z 43.10 100.00% 43 8000 83 6000

4000 111 I 111 174 ................ 423 m/ z 55.20 99.34% m/z-> 50 100 150 200 250 300 350 400 Abundance #4222:2-Trifluoroacetoxytridecane 43

5000 69

97 _uul m/ z 36.20 36.40 36.60 36.80 83.00 73.29% 1.1,4 119141. 182.......................................... n/z-> 50 100 150 200 250 300 350 400 Abundance #111573:1-Decanethiol

83 ' ■ i 1 36.20 36.40 36.60 36.80 5000 m/z 69.10 72.37% 29 112 140 174

li t—j—i—i—r—i—[—i

miz-> Abundance 50

57 83 100 150 200 250 #16349:1-Tricosene 300 350 400 A 1 ■ i ■ ■ 36.20 36.40 36.60 36.80 m/z 57.10 72.24% 5000 111 29

/z-> — 14h (l 50 H ■ 1139,169 100 196 224 252 , 294 322 . 1 । ■ 1 • 'i 1 1 11 /’TI ,"1 । 1 '• 150 200 250 300 350 400 A 36.20 36.40 36.60 36.80

10242.D SCAN020507.M Fri May 17 10:41:21 2002 Page 8

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