GCMS analysis results for sample AE10244, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020509\10244.D Vial: 22 Acq On : 10 May 2002 7:23 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS'Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.95 0.41 ug/1 48720 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

-1Phenanthrene-dl0 188 C14D10 001517-22-2 80 2 Anthracene-diO- 001719-06-8 72 188 C14D10 3 2,6-Naphthoquinone, 1,5-diamino- 188 C10H8N2O2 002783-59-7 50 43H-Pyrazol-3-one, 2,4-dihydro-4 , . . . 188 C11H12N2O 017694-06-3 46 Abundance Scan 4914 (31.952 min): 10244.D (-4901) (-) m/z 188.20 100.00% 188

5000

80 156

n/z-> TT 36,49.446, —Pmmm 92 132 146 ||| | T 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20 m/ z 80.10 20.49%

Abundance #79827: Phenanthrene-d 10 188

— 5000 31.60 31.80 32.00 32.20 m/z 156.10 13.45% 94 80 160 30 42 52 . 66 108118 132 146 II 170179|,| 11WTPTTTTTTTTH 11 TTTNTT11 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

31.60 31.80 32.00 32.20 5000 m/z 160.00 13.39%

p 80 94 1 60 17 30 42 52 00 , J 108118 132 146 I. 170179 ‘I miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79755:2,6-Naphthoquinone, 1,5-diamino- 188 31.60 31.80 32.00 32.20 m/z 184.20 12.94% 132 5000 160 104 =, 66 77 28 :39 51 ill 89 , 115 pmphm Ji 141. THTHtm TTTTTt । 169 11 Tt 111111 ■ ""i m/z—> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170180 190 31.60 31.80 32.00 32.20

10244.D SCAN020507.M Tue May 14 14:26:25 2002 Page 4

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