GCMS blank analysis results for VOCs, May 6-13 2002

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Data File : C:\MSDCHEM\1\DATA\02 0 513\0 5 0 6LB.D Vial: 3 Acq On : 13 May 2002 2:29 pm Operator: Nefliu Sample : 05/06 lab blk Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Phenanthrene-dlO Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.96 0.34 ug/1 39295 Phenanthrene- dl 0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1Phenanthrene-d10 188 C14D10 001517-22-2 86 2 Anthracene-diO- 188 C14D10 001719-06-8 80 3 -(A-Tolyl)-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 40 4 Pentacyclo [7.3.1.1. Abundance (4,12).0(2,7)... 188 C14H2 0 Scan 4916 (31.964 min): 0506LB.D (-4906) (-) 1000215-61-8 38 m/z 188.20 100.00% 188

5000

80 ' i ' ’ ' ' i 1 ' ' 1 1 1 1 1 1 I'1 Ton 1 1 ' 92 160 31.60 31.80 32.00 32.20 40 49 66 ( 112 133 X > | ! I I ! [ ! ! I I | I I I r | I I I'l |'tH I | I I I I | r i ) r t > i ) | I i । i । । DIT J i । i । PI I I | I ‘l r I | I I I I | I I if ] ‘l I I I | I | I I | I HTT m/ z 80.00 19.66% /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 31.60 31.80 32.00 32.20 80 m/z 184.20 17.63% 94 160 30 42 52 66 | I I ! T| I " I | ' I " I I I " | H-ll | I I I I RI ' I'l I " „4108118.132.146—179179—— n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

31.60 31.80 32.00 32.20 5000 m/z 189.00 15.97%

80 94 160 , 17 30 42 52 ° J J 108118 132 146 II 170179 । | । ' ' l j i i ' • | ' । i ' | । । । । | I । । i ] I I t i | > । I ' | I ' I I | I I । i | 1 1 I I | I I > I | II i i | I I I I | I I I I | I I I’H" I I | ITI I | I'r I T’TT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79716: -(4-Tolyl)-3-methyl-pyrazol-5-one ‘I i ' ' 1' । 1 n* ■' । 1 Ti i 1 188 31.60 31.80 32.00 32.20 91 m/z91.90 11.37% 105 5000

119

... 4151.J.78. + < I" " I" " I" ' I" " 1111 'I. I " " r 146 65 TTNIOUuTpT T’’ ' | T 1 ■ || ' 1 1 I 1 1 T I | I I I 1 | I

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

0506LB.D SCAN020507 .M Tue May 14 15:47:18 2002 Page 6

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