GC/MS analysis results, sample AE09684, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020507\09684.D Vial: 10 Acq On 7 May 2002 9:01 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Phenanthrene-dlO Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.36 ug/1 40632 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO 188 C14D10 001517-22-2 87 2 Anthracene-dlO- 188 C14D10 001719-06-8 81 3 Phosphonic acid, (3-methyl-3-pen... 188 C8H1303P 022152-34-7 53 4 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) ... 188 C14H20 1000215-61-8 49 Abundance • Scan 4916 (31.964 min): 09684.D (-4906) (-) m/z 188.15 100.00% 188

5000

80 1 । f । 1 ■ 1 1 । 1 1 1 1 । 1 1 1 1 । 1

1 ' 1 1 I1'1" 52 , 108 , 158. .1 495 31.60 31.80 32.00 32.20 m/z 189.20 23.37% m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #79827: Phenanthrene-d10 188

5000 ■ I ' > ■ i“ | । ‘ T i । । । I । । । ' | 1 31.60 31.80 32.00 32.20

80 m/z 187.20 20.67% 160 30 52 „ 1Q2 132 J l................................. I I I I I i l l I I I r I I I 1 i 3 I I I I I I I I I I I I I I I 'I'" I I I I I I I I 17| I I I I I I m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #79826: Anthracene-d10- 188

31.60 31.80 32.00 32.20 5000 m/ z 80.10 20.38%

p 94 160 17-42-58441241L‘‘II‘‘*II‘‘I‘II‘II‘’*........... .. ' m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #79704: Phosphonic acid, (3-methyl-3-penten-1 -ynyl)-, dime... ,...................... 188 31.60 31.80 32.00 32.20 m/z 184.10 12.90% 5000 77

35 . 109 155

m/z-> 4 50 100 150 ' 200 I 1 1 1 1 i 1 1 1 ' i 1 1 1 ' I 1 1 1 ■ i ‘ 250 300 350 400 ■ 1 1 1 1 1 1 । 1 450 500 —' i f ■ 1 ' i 1 1 ' 1 i 1 1 r 1 i 1 ' 31.60 31.80 32.00 32.20

09684.D SCAN020507.M Tue May 14 08:40:43 2002 Page 6

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