GCMS reference standard results for sample AE11424, May 2002

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Reference standard analysis report for nitrosamines and benzene derivatives in sample AE11424 analyzed May 17-21, 2002.

NYC-WTC_000022516–000022525

Folder label: “GCMS X 5/17/12 A 5/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020521\11424.D Vial: 10 Acq On : 21 May 2002 5:16 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.32 ug/1 33469 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual —1 Anthracene-diO- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 78 3 Cyclohexanone , phenyl hydra zone 188 C12H16N2 000946-82-7 50 4 Naphthalene, 1,7-dimethoxy-_________ 188 C12H1202 005309-18-2 43 Abundance - Scan 4915 (31.958 min): 11424.D (-4906) (-) m/z 188.20 100.00% 1168

5000 /................................. — 80 92 160 51 66 .II 3160 31.80 32.00 32.20 0 7 1 . T I | ITT. | . Il ompadlaadhhe > > i ■ • > 11 ■'111111 *l'1'11" I’T m/z 184.00 20.96% n/z-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79826: Anthracene-d10- 188

5000 1I 1 1 I ‘ 1 1 1 1 '' 1 1 1 ' 31.60 31.80 32.00 32.20 m/z 187.30 19.68% RR 80 94 160 . 17 30 42 52 P . I 108118 132 146 I. 170179b 0 1-r. , ! | F! . ! | , T, I | I I 1 . | I I 1 1 | I I I ) | I I I I | I FT l| I It. ] 1 111 J ■ . . I j > , , ■ [ I I I . [ F. I . | I > ′′′ . . I | ! ! . . | I’l’l" 1111 m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 * i 1 ■ 1 1 i ■ ' ■ ■ । 1 1 ■ ■ । • 31.60 31.80 32.00 32.20 5000 m/z 189.20 17.21%

80 94 160 30 42 52 66 , ,) 108118 132 146 I 170179b | 0-TI—m011—0011——000—00——m—pd—au——mmmhtmH n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance‘ #79722: Cyclohexanone, phenylhydrazone 188 31.60 31.80 32.00 32.20 93 m/z 160.10 16.34%

5000 55 65 41 77 106 . 145

m/z—> 0 TI-p-t 29 III 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Tmttmm 120 132 । 159 170 4 31,60 31.80 32.00 32.20

11424.D SCAN020521.M Fri May 24 09:25:13 2002 Page 5

NYC-WTC_000022524

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NYC-WTC_000022539

Laboratory report of GCMS analysis for sample AE11426 conducted on May 29, 2002.

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