GC/MS analysis results, sample AE09767, May 2002

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Data File C:\MSDCHEM\l\DATA\020507\09767.D Vial: 14 Acq On 8 May 2002 12:57 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 6 Anthracene-dlO- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.33 ug/1 39417 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene -dl 0 - 188 C14D10 001719-06-8 83 2 Phenanthrene-diO 188 C14D10 001517-22-2 74 3 C lohexanone, phenylhydrazone 188 C12H16N2 000946-82-7 53 4 Bi nzene, 1-(1-cyclohexen-l-yl)-4... 188 C13H160 020758-60-5 52 Abundance Scan 4915 (31.958 min): 09767.D (-4906) (-) m/z 188.20 100.00% 188

5000 94

49 66 80 134 158 31.60 31.80 32.00 32.20 111'111'1'11'1'1 Hrpti |‘ll 1111111’ 11111'1, ' i" '11" " i " " r1" 111111"11'111" r " 111 m/z 94.20 33.43% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d1 fl- 188

5000 ■ I ' ‘ ' 1 I 1 ' ’ 1 1 1 ' I I 1 I I I I 1 31.60 31.80 32.00 32.20 80 m/z 92.10 17.86% 17 30 42 52 68 94 I 160 ,|, 108 118 132 146 I 170179/, 4-p-rTTp-rrrp-rTTTt-rrr|H^^ + I I I I I I I I I ITI’I > I P I I I P I I I I I I I I TTTtM’’ I II P I I I I l‘l I I I Illi

n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ———————— 31.60 31.80 32.00 32.20 5000 m/z 187.20 15.52%

80 94 160 30 42 52 66 11 108 118 132 146—4179179 4. i'1111'11 'i''111111' i11111111' i11H ।11 I I I I I I j I I l'l P I I I P I1"'I' n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ........................ .............. .. Abundance #79722: Cyclohexanone, phenylhydrazone 188 31.60 31.80 32.00 32.20 93 m/z 189.30 15.36% 5000 55 65 41 77 106 145 29 III TTmt i n 11 ha 111' —||—— 120 132 । 159 170 ‘p-rrr ■ i r. । r । . . . r । ' ' । । । -i-1 -i । । ' m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

09767.D SCAN020507 .M Tue May 14 08:42:35 2002 Page 8

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