GC/MS analysis results, sample AE09767, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020507\09767 .D Vial : 14 Acq On 8 May 2002 12:57 am Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Pyrazine, tetraethyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.33 ug/1 39648 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrazine, tetraethyl- 192 C12H20N2 038325-19-8 50 2 2,5 ihydrophosphole, 3-methyl-1... 192 C11H13OP 1000196-97-5 50 3 4-H roxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 50 4 Bitscanate 192 C8H4N2S2 004044-65-9 49 Abundance Scan 4767 (31.088 min): 09767.D (-4756) (-) m/z 192.10 100.00% 192

5000 96 49 70 82 146 160 'so'so 31.00 31.20 3140 211 --HHl+ll 119 TTTTTTTTTTTTTTTTT ' i" " I" " I" 111'1" I — "i'" "i m/z 191.20 33.80% mfe-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #80990: Pyrazine, tetraethyl- 192 177

5000 i । | । I I । | i i i i । i r i i । i i 1 41 30.80 31.00 31.20 31.40 67 m/ z 96.20 23.89% 29 53 . 81 93 107 121 133 149 163 TmmPTTTTTTTP m/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #80965:2,5-Dihydrophosphole, 3-methyl-1 -oxo-1 -phenyl- 164 1 1 i 1 ■ 1 ■ i 30.80 31.00 31.20 31.40 5000 99 m/z 146.10 15.54% 115 47 67 77 195 146 177 ft m/z-> TPWTTTTT 27 38 157 r 187mll ml, # 1443474114155,, tire r.... 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 r " ■ i" " i

Abundance #81030: 4-Hydroxy-3,5-dimethylcinnamic acid '' 1 1 1 1 1 1 I 1 1 1 1 1 1 1 1 1 192 30.80 31.00 31.20 31.40 m/z 70.00 12.78% 5000 175

.. 11 89 £ 63 117 145 45 il 77 105 ”7 135 I 163 ------■< । ii'ri । ffri 11111‘i 1 1111 Pi |'11 11 । ri । । [ tri 1111 r ' I'11' I' Ti 111 ’' I m/z-> 20 30 40 50 60 70 80 90 100110120130140150160 170180 190 200 210 30.80 31.00 31.20 31.40

09767.D SCAN020507.M Tue May 14 08:42:33 2002 Page 7

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