GC/MS analysis results, sample AE09767, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020507\09767.D Vial: 14 Acq On 8 May 2002 12:57 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 4 Cyclopentasiloxane, decamet... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 15.46 5.55 ug/1 606051 Naphthalene-d8 16.53

Hit# of Tentative ID 5 MW MolForm CAS# Qual v 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 58 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 47 3 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 40 4 N-(Trifluoracetyl)-Q,O' ,O''-tris.. . 495 C20H36F3NO4Si3 054135-51-2 38 Abundance Scan 2107 (15.459 min). 09767.D (-2095) (-) m/z 73.05 100.00% 73

5000 267 355 । । । । i । t । । r । । । । । i' J । 1

45 15.20 15.40 15.60 15.80 103 TWPTTOOTImummmuur I ′| ■ । 293 323 133 154 | 111 ■ ■.. ।■ 7111 'r'l 1111111 193 223 249 m/z 267.00 30.44% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #115273: Cyclopentasiloxane, decamethyl- 73

5000 267 ■ ■ i ■ ■ 15.20 15.40 15.60 15.80 355 m/z 355.10 29.15% 45 28 111 96 115133 165 , 193 223 23 249 | Tf. Li . 11, ‘ T‘ rn 11 1 1 | 1 " ' I " t"i 11 ’ i'i ("1 T‘ i ¥-■ j i“i-i TT ' " I'l ' Ti | 293 323 ' | " 1 ' | 1 ' ‘ ' I1 ' ' 'I mlz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #115315: Cyclopentasiloxane, decamethyl- 73 ■ 1 i ' 1 1 I ' • ' ■ I ' ' 355 15.20 15.40 15.60 15.80 267 5000 m/z 356.10 12.70%

45 207 249 323 , | ' i " 1' i " " i " 11 r " ‘ i' " r r ■ " i" " r ■ ■11" " i ' " i11" i " " i' ' r " 11" ■11' ■ "i11 iTi TTT m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #115313: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... ■ ■ i 1 ■ ' 1 I ' ' ' 1 I ' 1 73 15.20 15.40 15.60 15.80 m/z 268.00 8.94% 5000 355 44 ! 93 130147 193 220237 267 294 | 384 mtt0000 ——mmma——muDTROgnp '1' I'1 ,Tr " ■ i'1 ■ mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 15.20 15.40 15.60 15.80

09767.D SCAN020507.M Tue May 14 08:42:31 2002 Page 6

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