GC/MS analysis results, sample AE09768, May 2002

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Data File C:\MSDCHEM\1\DATA\020507\09768.D Vial: 15 Acq On 8 May 2002 1:56 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 5 Cyclopentasiloxane, decamet... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

15.46 1.58 ug/1 155938 Naphthalene-d8 16.53 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 2 N- ifluoroacetyl)-N,O,O‘ ,0''-t... 553 C22H42F3NO4Si4 1000072-26-7 47 3 Phenethylamine, N-methyl- .beta. , . . . 399 C18H37NO3Si3 010538-85-9 38 4 Cyq opentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 35 Abundance Scan 2107 (15.459 min): 09768.D (-2094) (-) m/ z 73.05 100.00% 73

5000 355 267 - 15.20 15.40 15.60 15.80 45 103 — i rr 133 163 193 237 i -i ■ r—|-■■ ■ -1 f "ii 1*fII 325 1 m/z 355.00 41.84% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #115315: Cyclopentasiloxane, decamethyl- 73

355 267 5000 15.20 15.40 15.60 15.80 m/ z 267.00 32.91% 45 207 323 TTI——TRTT i r "ni 1 1 f । m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #27961: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethyls... 73

‘ I’’ ■ ■ । ■ 355 15.20 15.40 15.60 15.80 5000 m/ Z 74.10 11.76%

45 — „ 116 147 193 236 267 .......... 538 1 ‘ i ' ' ' ' 'i ' ' 1 ' i ' 1 ' ' i 1 '■ ' ' i 1 ' ' 1 i ' n/z- > 50 100 150 200 250 300 350 400 450 500 550 Abundance #115313: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... A 73 15.20 15.40 15.60 15.80 m/z 357.10 9.76% 5000 355

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1 . 116 147 , 193 220 , 267 294 .. 384 .............. ----- m/z-> 50 100 150 200 250 300 350 400 450 500 550 15.20 15.40 15.60 15.80

09768.D SCAN020507 .M Tue May 14 08:43:01 2002 Page 7

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