GC/MS analysis results, sample AE09768, May 2002

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Analytical report for sample AE09768 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.

NYC-WTC_000043792–000043805

Folder label: “GCMS X 4/25/02 A 5/7/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020507\09768.D Vial: 15 Acq On 8 May 2002 1:56 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 6 Phenanthrene, 2-methyl- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

31.08 0.32 ug/1 35325 Phenanthrene- dl 0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene , 2-methyl- 192 C15H12 002531-84-2 59 2 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 59 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 59 4 Anthracene, 9-methyl - 192 C15H12 000779-02-2 45 Abundance Scan 4766 (31.082 min): 09768.D (-4758) (-) m/z 192.15 100.00% 192

5000 ________ /.. 96 51 66 . 146 30.80 31.00 31.20 31.40 11.1JI 1’ ’’1’1111117 1221 351 1111111'11111111111 1—10110001100011111100000numam m/z 96.0.0 22.19% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #125842: Phenanthrene, 2-methyl- 192

5000 A11 I1 ..... 1 1 1 1 1 1 30.80 31.00 31.20 31.40 l..... m/z 193.10 20.44% 96 , 39 63 81 1115 139 155 i111' i1' ' ■ 1 1 1 1111 r‘1 ’’’’I "" 11,1111' -11' 1111" r " 11 ■' " i " 111 " " I I ■ ■ '11'1'' I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #125856: Phenanthrene, 1-methyl- 192 U ' 1 1 1I!I 1 ' 1 ' 1 v A ' 1 I ' 1 30.80 31.00 31.20 31.40 5000 m/z 190.90 15.19%

96 PE 39 63 81 1 115 139. 1111 • 111 > ■ 11111 । itii 11 > ।'i 111! ।*| rii । |Ti i r| it m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #81033: Phenanthrene, 9-methyl- 192 ....... ■ ■ । 1...... | LA ■ 11 । । । । । । । 1"I" ' 30.80 31.00 31.20 31.40 m/ Z 81.90 12.04% 5000 I

39 63 81 2115 139 165, . ‘I‘‘‘‘I‘‘‘-111111—01100TTO1C-0VUITTTIIIT I’’ ' 1 | "‘ IIT’II i । i i । i i । » | > il i ) T I I T | I ' X ' ' I ' ' n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 30.80 31.00 31.20 31.40

09768 .D SCAN020507.M Tue May 14 08:43:03 2002 Page 8

NYC-WTC_000043803

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GC/MS analysis results, sample AE09767, May 2002 · Box DEP Box 25

NYC-WTC_000043779

Analytical report for sample AE09767 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.

1 shared topics · Same agency, volume and box · similarity 0.998