GCMS analysis results for sample AE10812, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020521\10812.D Vial: 18 Acq On : 22 May 2002 1:09 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 Phenanthrene, 9-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.24 ug/1 25056 Phenanthrene-dl0 31.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N60 000945-24-4 53 3 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 42 4 4-Nitrobenzoylacetone 207 C10H9NO4 1000130-56-3 36 Abundance Scan 4768 (31.094 min): 10812.0 (-4758) (-) m/z 192.10 100.00% 192

5000

160 |......................... 315........... 503 30.80 31.00 31.20 31.40 43 82 0t -- I ....................1, m/Z 160.20 18.82% m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #81033: Phenanthrene, 9-methyl- 192

5000 ■ 1 i ' ' ■ ■ i ' ' ■ i ■ ■ ■ ■ । ■ ■ 30.80 31.00 31.20 31.40 m/z 146.10 16.15% 96 O+r I3963,, T-f I* 1nI 139,155.4 n/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #125821:2,4-Diamino-6-(hydroxymethyl)pteridine 43 163 192 .... AA, 30.80 31.00 31.20 31.40 5000 m/z 193.00 14.54% 68

0+ 4414.22444/1/ n/z—> Abundance 50 100 150 200 250 300 350 #125842: Phenanthrene, 2-methyl- 192 400 450 500 1 ■ i ■ ‘ ■ i 30.80 31.00 31.20 31.40 .....I m/z 191.20 11.41% 5000

m/z-> 0 3^63,,^ 139/165.1 ..... ...... ...... 50 100 150 200 250 300 350 400 450 500 . .... Ili)... . 30.80 31.00 31.20 31.40

10812.D SCAN020521.M Fri May 24 09:21:54 2002 Page 7

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