GC/MS analysis results, sample AE09768, May 2002

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Data File C:\MSDCHEM\1\DATA\020507\09768.D Vial: 15 Acq On 8 May 2002 1:56 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 7 Anthracene-d10- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.35 ug/1 38898 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 83 3 3Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 43 4 Naphthalene, 2,6-dimethoxy-____________ 188 C12H1202 005486-55-5 37 Abundance Scan 4914 (31.952 min): 09768. D (-4904) (-) m/z 188.20 100.00% 188

5000

* ao 42 5 54 66i 80 | ।94 j 124 144 158 31.60 31.80 32.00 32.20 I I . . I > I . . I . I ! . > I l i'l > l‘l I 11 I I ri f I I I I . . I. I I I I 11. > | i I P [ i / | I | > i > I h । | i < I i j i I । i [ i ‘I m/z 184.20 16.18% lz-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160170 180 190 Abundance #79826: Anthracene-d10- 108

5000 / 31.60 31.80 32.00 32.20 m/ z 18 9.10 15.70% . 80 94 160 , |. 66

n/z-> 10 17 30 42 52 ■ । i । i । p > i । । i i i r| I i ■ i । I I i 'ii''11 ■','I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 108 118 । I | I । | f [ r 132 I । i i ii । I I I 146—44179179 — ‘ T Abundance #79827: Phenanthrene-d10 168 r , । ] > r 1il . l*T ] I I I I I I i I I | i

31.60 31.80 32.00 32.20 5000 m/z 80.20 14.01%

„ 80 94 160 ........... 30 42 52 9 1l .108 118 132 146 .[J 170179,1.1 I___ ' 111 11 ] 111' ।1 > 11 p 11 1111 <11 11" 111 11II 111 111111111 1111111111 > । 1111111 11111 rl'l |‘i rTTt 111111111111111 /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79771: 3-Amino-4-methyl-6-methoxyquinoline Tif । t . । . । r । ’II’ ■ ■ ■ [ ' । ' । p 168 31.60 31.80 32.00 32.20 m/z 66.10 12.35% 145 5000

41 51 63 77 89 102 117 11| 130 159 173 , ------------ r ’ p 1 1 IT r 1 TTi l I > I I I I I I I I /z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

09768.D SCAN020507.M Tue May 14 08:43:05 2002 Page 9

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