GCMS sample analysis results for unknowns, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020513\10068.D Vial: 25 Acq On : 14 May 2002 12:20 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.33 ug/1 31915 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 87 2 Phenanthrene-dlO 188 C14D10 001517-22-2 87 3 3H-Pyrazol-3-one, 2,4-dihydro-4,... 188 C11H12N2O 017694-06-3 50 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 50 Abundance Scan 4915 (31.958 min): 10068.D (-4906) (-) m/ z 18 8.10 100.00% 188

5000

160 ..50 64 84.94 'i । । । r । । । । । । । । । 11 । ^'i i । | 11 । । । । I । 11 । । । I । 111 11 ri r । i । । i 11 i । i । 11 132....... 11. .. .... .1,, 1.... 1,8 I I I I I I I I I I I I I I I I I I I I III I I III 31.60 31.80 32.00 32.20 m/ z 160.20 12.90% rn/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-dIQ- 188

5000 TF f’TIFIIIIII’ 31.60 31.80 32.00 32.20 m/ z 189.20 11.24% 80 94 160 , i, 17 30 42 52 66 J 108 118 132 146 ,|| 170179.1 i | i । ■ i | i i i I | I I I I | I I I I | I I H 1111111111 + 11 Hi ITTTT" in i । 11 it[ lit 111111 I I ’’’ 11 IJ 111111 llllllll Illi m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 0 31.60 31.80 32.00 32.20 5000 m/z .94.00 10.96%

80 94 160 30 42 52 66 rl i 11 11 Mt i i 11 i r i 11 i । i [ 11 i rpl i r ij 11 I 11 i I’l’l 11179179/,. | | । I I 1 | i I | I r I | H I i । । | । I । । I I । | I _ | | । 108 118 132 146 I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79695: 3H-Pyrazol-3-one, 2,4-dihydro-4,4-dimethyl-2-phenyl- 188 31.60 31.80 32.00 32.20 55 m/z 184.20 10.19% 77 5000

39 160 64 105 119 132 | 173 /........................ 111''' 11' 111 ‘ 111" -TT n<‘| M I I | I , I 145 1111 " i11 ■ 11 ■ । ■l■■ T’’ ' I f ' 1 1J 1 ' i-r | -i > i । । । i i । । ।

ti/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

10068.D SCAN020507.M Wed May 15 09:53:52 2002 Page 4

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