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GCMS blank results for sample AE11282, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing blank test results for GCMS analysis of sample AE11282 conducted between May 13 and May 16, 2002.

NYC-WTC_000024534–000024542

Folder label: “GCMS X 5/13/02 A 5/16/02

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NYC 9/11 Public Portal Document Library Search compound Report

Data File : C:\MSDCHEM\1\DATA\020516\0513LB.D Vial: 4 Acq On : 16 May 2002 12:20 pm Operator: Nefliu Sample : 05/13 lab blk Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Pyrazine, tetraethyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

31.09 0.21 ug/1 17470 Phenanthrene- dl 0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrazine, tetraethyl- 192 C12H20N2 038325-19-8 9 2 Anthracene, tetradecahydro-, (4a... 192 C14H24 001755-19-7 9 3 Benzene, 1,1'-(1,2-propadienylid... 192 C15H12 014251-57-1 9 4 9-Borabicyclo[3.3.1]nonane, 9-(l... 192 C13H25B 136704-93-3 9 Abundance Scan 4768 (31.094 min): 0513LB.D (-4758) (-) m/z 192.10 100.00% 1912

5000

96 146 160 | 30.80 31.00 31.20 31.40 44 66 84 11"'' i1"1111" r11111111' i" " i11" i1 TmOTTTTTTTTTTTTTTTTTT " i" m/z 193.20 30.65% /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80990: Pyrazine, tetraethyl- 192 177

5000 1-1 | 1 1 1 ' | 1 । 1 I ' ' ' ' I ' ' 41 30.80 31.00 31.20 31.40 67 m/z 191.10 22.06% 53

z-> M 29 81 , || 93 Tmmmmmmmmp 107 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 121 133 149 i 163 I T 1 ■ i ‘ ■

Abundance #80932: Anthracene, tetradecahydro-, (4a.alpha.,8a.alpha.... 19/2 135 ■ ■ i ■ ■ 30.80 31.00 31.20 31.40 5000 67 m/ z 96.20 21.50% 81 95 55 121 150

l... 110 .. I .... I TTTt I 163 177 n/z-> Abundance ' i ■ ■ •1 r " ' r 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #125850: Benzene, 1,1'-(1,2-propadienylidene)bis- 1 2 ‘" i"

.... n.... 30.80 31.00 31.20 31.40 m/ z 95.30 12.52% 5000

165 115 26 39 51 63 74 33.34 103 'I"''!" nmhpmI | i 126 139 | | I I 11 | I I m'| I 152 -, TH 176 gur 1 ' i ' 1 ' 1 i ' i 1 ■ ' 1 i ■ ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 30.80 31.00 31.20 31.40

0513LB.D SCAN020507.M Fri May 17 10:30:06 2002 Page 4

NYC-WTC_000024540

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NYC-WTC_000024540Source: NYC Law Department, mirrored locally

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