GC/MS analysis results, sample AE09769, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020507\09769.D Vial: 16 Acq On 8 May 2002 2:55 am Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Phenanthrene-dlO Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.36 ug/1 40977 Phenanthrene-dl0 31.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO 188 C14D10 001517-22-2 59 2 Anthracene-d10- 188 C14D10 001719-06-8 50 3 1, 4-Naphthalenedione, 2-hydroxy-... 188 C11H803 000483-55-6 38 4/3H-Pyrazol-3-one, 2,4-dihydro-4,... 188 C11H12N2O 017694-06-3 37 Abundance Scan 4913 (31.946 min): 09769. D (-4905) (-) m/z 188.20 100.00% 188

5000

80 94 160 TTT |11***IIIII 31.60 31.80 32.00 32.20 40 . 54 66 112 132

mlz-> mp 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 TIT 11' ■ <' 1111 ■ । < ... M...... # I’T m/Z 184.10 28.95% Abundance #79827: Phenanthrene-d10 188

,........................ 5000 31.60 31.80 32.00 32.20 m/z 189.20 24.00% 80 94 160 30 42 52 66 I I I I I I I I IFITTFI 1111111 mrfmrttrt’i T t j TTft 108.118.132,146..1,-179,179..— n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 TTT i 1 ■ ■। 1 1 1 ■' i 1 1 1 r i 1 31.60 31.80 32.00 32.20 5000 m/z .94.10 19.61%

RA 80 94 160 | 17 30 42 52 ° ,| ,| 108 118 132 146 ,|| 170179. TETTTTTTTTTTTTTTTTTTHTTTTTTTHTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT+ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125707:1,4-Naphthalenedione, 2-hydroxy-3-methyl- "tT IITIa‘I‘11 188 31.60 31.80 32.00 32.20 m/ Z 160.20 16.71%

5000

50 77 105 131 160 ' i ■ " ■ i ‘1" i ■1" i" " I'"'' ............ mm....... . ................. .. ........ nnlr-xp,,,,,,. ----- T’T m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

09769.D SCAN020507.M Tue May 14 08:43:34 2002 Page 8

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