GC/MS analysis results, sample AE09769, May 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020507\09769.D Vial : 16 Acq On 8 May 2002 2:55 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 Bitoscanate Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 31.08 0.32 ug /1 37310 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Bitoscanate 192 C8H4N2S2 004044-65-9 52 2 Bitoscanate 192 C8H4N2S2 004044-65-9 52 3 Bitoscanate 192 C8H4N2S2 004044-65-9 52 4 1,5-aphthalenedithiole 192 C10H8S2 1000223-69-5 50 Abundance / Scan 4766 (31.082 min): 09769.D (-4755) (-) m/z 192.10 100.00% / 192 A

5000

146 160 44 64 82 94 ng 30.80 31.00 31.20 31.40 < > | > ! I ! [ ! I > I | I I ! ! | ! ! I ! | 111 I |' | | I | | | | r I'pr I I I | l‘ I I I | | I I | | !r I ! | | | I | | | , | | | | I’r 11" " ■ i" " ir"11 T’T m/ z 160.20 20.34% m/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #125827: Bitoscanate 192

5000 1 ■ i 1 1 1 ' i 1 r 134 30.80 31.00 31.20 31.40 50 63 75 90 160 m/z 146.10 19.83% 4 1428 28 1 l+. IHThr 102 116 ttd Bp i i | i | i I | I II i । i i II । I । t I 11 | | I I 148 n/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80930: Bitoscanate 192 .......... I A.......... ' 1 i ' 1 1 ■ i 1 ' 11 । 1 । ' । । । । 30.80 31.00 31.20 31.40 5000 m/z 191.10 19.42%

_ _Q 50 26 39 , I, , 1 iti,| III i i'll( rTTp 1* । > 11 > 11111 r 11111 < '111111 r 1111 1 107 .122 , 63 75 148 160

NITPelyunnnjui 90 134

I— — t n/z—> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #125828: Bitoscanate ........... I I.................. 192 30.80 31.00 31.20 31.40 m/z 193.00 16.11% 5000 134 160 4--4++H4 +++90,102 122 r nm ... 50 148 176 63 75 II’T ■ i ■ । ■ 11 <" 11" THTTT Tl’n ri 11'| 11111'| 11 /z—> o 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 30.80 31.00 31.20 31.40

09769.D SCAN020507.M Tue May 14 08:43:32 2002 Page 7

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