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GCMS analysis results for sample AE08253, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08253 conducted on April 19, 2002, including surrogate recovery data.

NYC-WTC_000047830–000047850

Folder label: “GCMS X 4/8/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\O2O417\O8253.D Vial: 11 Acq On : 17 Apr 2002 5:42 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 Bitoscanate Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 22.64 0.31 ug/L 487886 Phenanthranene-dl0 23.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Bitoscanate 192 C8H4N2S2 004044-65-9 50 2 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 50 3 Bitoscanate 192 C8H4N2S2 004044-65-9 47 4 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 47 Abundance Scan 3330 (22.645 min): 08253. D (-3323) (-) m/z 192.10 100.00% 192 |

5000 . ................. 82 96| 92 146 160 | 22.40 22.60 22.80 23.00 42 52 66 120 0 I " I" " I I |'I ! I I ] I f I I [ I I I I | I I H | "tFr/ I I I I | I I I I | ++ .I. I | i H'l । i i > I |‘i i r i । r i i I | ! । I I ’ 1111 m/ Z 191.10 21.86% m/z—> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80930: Bitoscanate 192

5000 22.40 22.60 22.80 23.00 134 90 160 m/z 146.00 15.31% 26 39 50 63.75 O-T TPm 148 pl r i ! 11,1 TTTTTTT " r "' i11" i I 107’ I 11122 Thrrrrrt n/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80950: 1,5-Naphthalenedithiole 192 .......... / 1 i 11 ■ 1 i 11 22.40 22.60 22.80 23.00 5000 m/z 193.10 14.15% 115 128 159 40 57 69 79 96 147

/z-> O-T 0 Hmm yrkpn 117 177 11 i" 1‘II" 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #125827: Bitoscanate 192 22.40 22.60 22.80 23.00 m/z 96.00 13.23% A 5000 134 90 160 A 50 63 75

m/z-> 4 14 29 39 0 117 1‘T , ,^1,41'., 'l )+# +++ I I I 1 148 I 1I I I f II 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 r1111"111 .te. ________ _______ ' 1 1 1 1 1 1 1 1 1 1 1 1 1 1 ' '*1 22.40 22.60 22.80 23.00 '

08253.D 041702SCAN.M Fri Apr 19 08:38:02 2002 Page 11

NYC-WTC_000047844

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NYC-WTC_000047844Source: NYC Law Department, mirrored locally

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