GCMS analysis results for sample AE08253, April 2002

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Laboratory report documenting GCMS analysis of sample AE08253 conducted on April 19, 2002, including surrogate recovery data.

NYC-WTC_000047830–000047850

Folder label: “GCMS X 4/8/02 A 4/17/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08253.D Vial: 11 Acq On : 17 Apr 2002 5:42 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.53 ug/L 838849 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO - 188 C14D10 001719-06-8 87 2 Selenide, ethyl 1-methyl-l-pente... 188 C8H12Se 025128-48-7 52 3 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 38 4 5-Oxazolecarboxamide , 2-phenyl- 188 C10H8N2O2 039819-42-6 38 Abundance Scan 3420 (23.174 min): 08253. D (-3414) (-) m/z 188.10 100.00% 188

5000

mfe-> Abundance 43 57 66 80 0- ------ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 108 132 146 160 170 f । । I । । । । । । riTi 11 । I । । i । I । । i । PPPri’m । | i i i t1

#79826: Anthracene-d10- + 22.80 23.00 23.20 23.40 23.60 m/z 94.10 19.13%

188

5000 TT । 1 1 1 1 । 1 22.80 23.00 23.20 23.40 23.60 m/z 189.10 13.63% 80 94 160 . 66

m/z-> 0 17 30 42 52 I | I I I I | I I I I--- TT I [ I i । | | | i r r | । I > I | I I I I | II i

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 , 108 118 132 I f | I I It I 1 II [ I I I V| I I I I | I I I „146—+170179—— TI

Abundance #79821: Selenide, ethyl 1-methyl-1-penten-3-ynyl 188 --- 22.80 23.00 23.20 23.40 23.60 5000 m/z 184.05 12.27%| 79 159 145 173 A l 0 । [ । । । । । i > । i p"i । । । । । । i | । ! । । | । i i i । rt 91 107 119 131 j > । । ' । । > । i [ r r I I'l’t-rd | । । i i ■ |* i • | i IT 1) m/z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy- oxime 188 "I n IT 22.80 23.00 23.20 23.40 23.60 m/z 80.10 10.77% 5000 143 _ 89 115 51 0 rr I ! I | I M , ! I I I I | . I M |‘l I I , 64 76 I 102 , 130 | I I 4rt r | I t1' I | I I | | I I I’ | | /‘III Ji 158 170 mP mn I I I 1 I L L I I- I I I I I I _ I I I I

/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40 23.60 | .

08253.D 041702SCAN.M Fri Apr 19 08:38:05 2002 Page 12

NYC-WTC_000047845

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NYC-WTC_000047845Source: NYC Law Department, mirrored locally

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