GCMS results sample AE08254, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \MSDCHEM\ 1 \DATA\ 020417\08254.D Vial: 12 Acq On 17 Apr 2002 6:32 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

23.17 0.69 ug/L 1165580 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 3 5-Oxazolecarboxamide, 2-phenyl- 188 C10H8N2O2 039819-42-6 40 4 Phenanthrene-dlO 188 C14D10 001517-22-2 38 Abundance Scan 3420 (23.174 min): 08254 D (-3413) (-) m/z 188.10 100.00% 188

5000

94 43 57 66 80 22 80 23 00 23 20 23 40 23 60 108 132 160 -n/Z-> 0- 111 (•i'i 1111 ll+++ [ ■ 111 fi 11 ij> i'h| I 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 "I'.... rnrt '"n '"I ■ 11'1''' I " m/ z 94.00 18.53% Abundance #79826 Anthracene-d10- 18 8

5000- 22 80 23 00 23 20 23.40 23.60 m/z 189.10 16.89% RR 80 94 160 | 17 30 42 52 ° | | 102 118 132 146 | 170 1801, 01 » | I 1 ■ i | | i i i | ; i i । | 11 i । । I I । । । 11 | । । i । | | 11 । । 1 | | | ] >| t 1 । । । ( i । । । । । 11 । | । । । । । । | nt4’i r i | | 11 | | | IM 41 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79771 3-Amino-4-methyl-6-methoxyquinoline 108

145 22 80 23 00 23.20 23.40 23.60 5000 m/z 184.10 12.89% A 117 41 51 63 7 7 89 102 1 30 0 ' i1" 11' " ' i1 " ■ i'1, ■ | 1 rill-i qrulrpo i rl, 11 n’r । rilly 11 4 n 11 il, 11 173 IL ml159ivimnonpond 115’ ‘ ‘I n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79737: 5-Oxazolecarboxamide, 2-phenyl- ‘IT 116 108 22 80 23.00 23 20 23 40 23.60 144 m/z80.10 8.46%

5000 89

28 39 51 77 105 | n/z--> 0 l " " 1111,11' " 11 1111"1 rl 1 ■ i" " ।। ■ 1' i' " 11" " r " ' r 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 mm TBit 22.80 23.00 23.20 23 40 23 60

08254.D 041702SCAN.M Thu Apr 18 09:23:29 2002 Page 9

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