GCMS analysis results, Sample AE08262, April 22, 2002

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GCMS analysis report for sample AE08262 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048309–000048332

Folder label: “GCMS X 4/9/02 A 4/17/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\l\DATA\020417\08262.D Vial: 19 Acq On 18 Apr 2002 12:18 am Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 11 Anthracene-dlO- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 23.17 0.55 ug/L 812447 Phenanthranene-dl0 23.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 93 2 Phenanthrene-diO 188 C14D10 001517-22-2 80 3 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 47 4 3,4-Oxazolidinecarboxylic acid, ... 245 C11H19NO5 116842-10-5 47 Abundance Scan 3420 (23.174 min): 08262.D (-3411) (-) m/z 188.10 100.00% 18 8

5000 ..... / 1 1 ‘ 1 ‘ 1 I '

40 57 66 80 34 136 146 160 |. 22 80 23 00 23 20 2340 23.60 0 ----- fmm m/z 189.15 14.75% /z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 118

5000 22.80 23.00 23.20 23.40 23.60 m/z 184.10 13.17% 80 94 160 . I 66

n/z—> 17 30 42 52 ov......................... 10 mH +179,1294 4"0 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ! 118 132 ■111"111 ■11111111"111 146

Abundance #79827 Phenanthrene-d10 118 . . । .^T . 1-| I I I > | I I I I | I 22 80 23.00 23.20 23.40 23.60 5000 m/ z 94.05 12.75%

80 94 160 66 0-pm 30 42 52 ‘ 1 102110118 132 146 170 180 | r1 ■ ■ ■!m > .|■! | | 11 i rl 11 I I P I i i | 111 I I 11 11 I M 11 11 n F] 1-1 tT | TTTTTTT n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79739: Cycloheptanone, 4-phenyl TI TT 188 22 80 23 00 23 20 23.40 23.60 117 104 m/z 80.05 11.09% 91 160 5000 131 170

27 39 51 65 78

/z- > 0-T -llll44, 4+ — M 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 L 22.80 23.00 23.20 23.40 23.60

08262.D 041702SCAN.M Thu Apr 18 09:49:33 2002 Page 16

NYC-WTC_000048327

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