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GCMS analysis results for sample AE08253, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08253 conducted on April 19, 2002, including surrogate recovery data.

NYC-WTC_000047830–000047850

Folder label: “GCMS X 4/8/02 A 4/17/02

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Scanned page image, NYC-WTC_000047846
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08253.D Vial: 11 Acq On : 17 Apr 2002 5:42 pm Operator: Nefliu Sample : sample • Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 8 2-Iodoethyl laurate Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.46 0.33 ug/L 443654 Chrysene-dl2 30.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Iodoethyl laurate 354 C14H27IO2 1000117-50-2 27 2 Benzoic acid, p-anilino-, methyl... 227 C14H13NO2 004058-18-8 12 3 Furo[3,2-b]pyridine, 2-methyl-, ... 149 C8H7NO2 069022-83-9 10 4 1,2-Benzenedicarboxylic acid, mo... 278 C16H2204 004376-20-9 10 Abundance Scan 4830 (31.458 min): 08253.D (-4823) (-) m/z 227.10 100.00% 227

m/z-> 5000

Abundance 0 40

40 57

1111133... 85 113 149

167 207

। । । I । ' । > ' । । । । r |~1 r r । । । । i r'| । । । i । i । । । । r । ■ i । । । i । i । । TTTUuTTT 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #89029: 2-lodoethyl laurate 227 ' 1 I 1 11 1 I ' y. 31.20 31.40 31.60 31.80 m/z 149.00 66.11%

43 155 5000 .............. I h 111111' ।1'11 I r 31.20 31.40 31.60 31.80 71 97 m/z 40.00 50.40% 183 200 354 0 ‘‘i 44 T< i | I i i । J | । i r | i i i r । > i — TI——mmu—*n‘u—nmm‘andngr m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #89099: Benzoic acid, p-anilino-, methyl ester 227 196 । । । । । । i ] । i । । । । । । । [ । ■i 31.20 31.40 31.60 31.80 5000 m/z 113.60 48.41% 167 _ 77 98 51 77 I 115 139 01 I I I fl 4m++ 1 . p dmt r+) I ! I | |4, I | l I I ,l I ■1 ■11'11111 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #66755: Furo[3,2-b]pyridine, 2-methyl-, 4-oxide 149 II 1..... ' 1 I 1 1 ' ' I 1 1 f 1 [ ' I I 1 I I I 31.20 31.40 31.60 31.80 m/z 57.00 33.29% 5000

/z-> 43 11 o > ■ i ■ ill 40 66 I ■11 i ■ ■ ■ • । ■ 60 104 1 133

1 ■ i111111 ■1' i ■ ■ ■' 111 ■ ■ i1 ■' ■ r ■ ■ ■ i1111 (111' i'1111111111 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.20 31.40 31.60 31.80

08253.D 041702SCAN.M Fri Apr 19 08:38:08 2002 Page 13

NYC-WTC_000047846

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NYC-WTC_000047846Source: NYC Law Department, mirrored locally

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