GCMS analysis results, Sample AE08264, April 22, 2002

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Data File : C:\MSDCHEM\1\DATA\020417\08264.D Vial: 21 Acq On : 18 Apr 2002 1:56 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 13 Benzoic acid, p-anilino-, m.. Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T.

31.45 0.35 ug/L 549266 Chrysene-dl2 30.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, p-anilino-, methyl... 227 C14H13NO2 004058-18-8 35 2 Benzoic acid, 3-(phenylamino)-, ... 227 C14H13NO2 055622-43-0 25 3 Phthalic acid, diisooctyl ester 390 C24H3804 001330-91-2 25 4 1,2-Benzenedicarboxylic acid, mo.. 278 C16H2204 004376-20-9 16 Abundance Scan 4829 (31 452 min): 08264.D (-4822) (-) m/z 149.00 100.00% 149 227

5000

0- 40 57 71 85 99 113

1 167

197 236 j’.......... | | — 31.20 m/z 227.20 A 31 40 31.60 31.80 88.77% n/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #89099: Benzoic acid, p-anilino-. methyl ester 2; 7 196

5000 — 167 31.20 31 40 31 60 31.80 m/z 40.00 44.21% 41 51 65 77 98 n/z- > 04 ' 11* ' 40 60 '.. 1,482.1, --- 80 120 100 140 115 128 139 11, 180 r 1 p • « i1' 160 180 T 200 L 220 240 Abundance #89078: Benzoic acid, 3-(phenylamino)-, methyl ester 227

31 20 31 40 31.60 31.80 5000 m/z 167.00 34.52% 167 196 52 66 77 89 98 139115 0- • • i 1 ,4, । I’’■ 1 1 i । . ■ । ' > n* i 1 * 1 f I‘ ‘TT 182 |. n/z- > 40 60 80 100 120 140 160 180 200 220 240 Abundance #66787 Phthalic acid, diisooctyl ester TIT II, 149 31.20 31.40 31 60 31 80 m/z 57.00 30.79% 5000 57 167 43 71

/z-> 0- 40 60 83 113 I 95 144 , । ’T . 80 || 122132 ‘1 । -1* । 'I1, । I"I r i । । i1 100 120 140 160 180 200 220 240 i.. l>... 31 20 31.40 31 60 31.80

08264 .D 041702SCAN.M Thu Apr 18 09:52:46 2002 Page 18

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