GCMS analysis results for sample AE08251, April 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08251.D Vial: 9 Acq On : 17 Apr 2002 4:02 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L

Peak Number 20 1,2-Benzenedicarboxylic aci... Concentration Rank 19

R.T. EstConc Area Relative to ISTD R.T.

31.46 0.24 ug/L 271464 Chrysene-dl2 30.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, mo... 278 C16H2204 004376-20-9 22 2 Phthalic acid, diisooctyl ester 390 C24H3804 001330-91-2 22 3 1,2-Benzenedicarboxylic acid, mo... 278 C16H2204 004376-20-9 10 4 N-Benzylbenzenecarbothioamide 227 C14H13NS 014309-89-8 9 Abundance Scan 4830 (31.458 min): 08251.D (-4824) (-) m/z 149.00 100.00% 149 227

40 5000- 57 167

ux . 1.. 1.... i|.T... 70 86 113 197 31.20 31 40 31 60 31 80

N 0) I 1 1 1 1 F1+r m/z 227.05 97.13% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #67064 1.2-Benzenedicarboxylic acid, mono(2-ethylhexyl) este 149

5000 31 20 31 40 31 60 31.80 70 167 41 , m/ z 40.00 56.80% 29 । 55 83 112

n/z- > 0+TTT 20 12,14/4/1.270.1,*—* 40 60 80 100 120 132 140 160 185 199 213 228 242 256 11‘y1‘*s11‘II****‘1**.‘***G* 180 200 220 240 260 278 280 Abundance #66787 Phthalic acid, diisooctyl ester 149 TTT । ■ ■ ■ ■ । ■ • 31 20 31.40 31 60 31.80 5000 m/z 41.00 36.94% 57 167 43 71 83 07 113 — — TVZ—> 0 20 40 60 .4.8711,121, 80 100 120 140 160 180 200 220 240 '111111111 ■ ■' । ■''' ।'1' ■ । ■ ■' ■ ।1'

260 280 Abundance #123456: 1 2-Benzenedicarboxylic acid, mono(2-ethylhexyl)... 149 31 20 31 40 31 60 31.80 m/z 57.10 35.93% 5000 70 57 167

LIL -+ it....... .. 41 83 112

0 279 Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 31 20 31.40 31 60 31.80

08251.D 041702SCAN.M Thu Apr 18 09:12:19 2002 Page 25

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