GCMS analysis results for sample AE08251, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08251.D Vial: 9 Acq On : 17 Apr 2002 4 : 02 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 19 Phosphonic acid, dioctadecy... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.07 0.90 ug/L 1031130 Chrysene-dl2 30.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9 92 2 l-Docosene 308 C22H44 001599-67-3 62 3 2-Propenoic acid, n-pentadecyl e... 282 C18H3402 1000245-64-0 53 4 Dodecyl acrylate 240 C15H2802 002156-97-0 47 Abundance Scan 4424 (29 073 min): 08251 D (-4415) (-) m/z 55.10 100.00% 55

5000 69 83 97 4 111 127 —1 + IM?/*n Mr 28.80 29 00 29.20 2940 0 - A1 1..00./1,,44.141 ______ m/ z 43.10 45.73% n/z—> 20 40 60 100 120 140 160 180 200 220 240 260 280 300 80 Abundance #13890 Phosphonic acid, dioctadecyl ester 56 69 83 4 97

5000 MAMwAAihAp MMA—MAMC 111 28.80 29 00 29 20 29.40 136 m/z 57.10 44.60% A n/z-> ol 1,24.4.4,../ +14+151 20 40 60 80 '' i' ■ 11 i ■' ■ ‘ i ' ■ ■' i ■ ■ 100 120 140 160 180 200 220 240 260 280 300

... Y Abundance #111438. 1-Docosene 4 53

69 83 97 I*....... 28 80 29 00 29 20 29.40 5000 m/ z 83.10 42.05% 111 125 14 । , I 139 153167181 308 0+ ’ । iri rp । ’II rr u.d.m 1 idij ri .. 11 > 1 < । i > i > । i < ! i । i । । i । i । । i । n/z- > 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance 55 #13489. 2-Propenoic acid, n-pentadecyl ester 4-—r 28.80 29 00 29.20 29.40 m/z 69.10 41.27%

5000 4 73 97 111 127 0 ’III , ,14,4+ 44.4.4.4 TTOTuummgUDTPTPTTT 140153166 182 210 1 । i - < ■ i ■ ‘ n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 28.80 29.00 29.20 29.40

08251.D 041702SCAN.M Thu Apr 18 09:12:19 2002 Page 24

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