GCMS analysis results for sample AE08425, May 2002

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Laboratory report documenting GCMS analysis of sample AE08425 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048148–000048168

Folder label: “GCMS X 4/9/02 A 4/19/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020419\08425.D Vial: 12 Acq On : 19 Apr 2002 6:58 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 8 1-Heneicosyl formate Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

38.55 15.88 ug/1 27374800 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 l-Heneicosyl formate 340 C22H4402 077899-03-7 76 2 1,2-Octadecanediol 286 C18H3802 020294-76-2 72 3 Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9 70 4 E-15-Heptadecenal 252 C17H320 1000130-97-9 68 Abundance Scan 6036 (38.544 min): 08425. D (-6028) (-) m/z 55.10 100.00% 55 A 83 5000 ) I 111127

/z-> " 111" r 1111 4AA | Ai . 153169 197 225 1 11T ’ .-P ITTImmi I TTi ITTErTu I 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 252267 295 324 I I I I | I I | I | I! ! 1 ! I I I I | ! I I 1 | I I 38.20 38.40 38.60 38.80 m/ z 57.10 54.26% Abundance #16592:1 -Heneicosyl formate 57 83 ................................... ..... ..............

5000 4 111 38.20 38.40 38.60 38.80 m/z 43.20 53.78% —LL '11'''1 I'' “I' , 1 139154 TIPI 182 210 266 294 322 340 " i" " i" • ■ i " " i" ■' i" " i ■ ■ " i1 ■ rn/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #16347:1 2-Octadecanediol

4 57 83 ...... R.... -... 38.20 38.40 38.60 38.80 5000 m/ z 83.10 52.80% 111 18

m/z-> ...... . 20 40 AL ,4132154 TIUTIIuumuuuguu 182 207224 255 281 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #13890: Phosphonic acid, dioctadecyl ester ■ ■ i 1 ■ 1 ' i ' ' 1 ■ T1 1 ' 1 i ■ ’ 5 83 38.20 38.40 38.60 38.80 m/z 73.10 46.34% 5000 111 29 136 I I, J, 151.............................................. 1‘ 11111111110101111019""0 ‘00-0‘0110—00‘00‘070uO—TT"‘tI0r ...................... / ITT’’ । ■ I > 1 ' I ' ■ ' 1 r1 ' ' /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 38.20 38.40 38.60 38.80

08425.D SCAN020418.M Thu May 02 15:28:12 2002 Page 10

NYC-WTC_000048161

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