GCMS analysis results for sample AE09571, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\l\DATA\050902\9570.D Vial: 7 Acq On 9 May 2002 8:10 pm Operator: Mclean Sample 5/8 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 7 Heneicosane Concentration Rank 20 R.T. EstConc Area Relative to ISTD R.T. 29.18 1.38 ug/L 2400500 Chrysene-dl2 30.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 38 2 Octadecane 254 C18H38 000593-45-3 38 3 Heptadecane 240 C17H36 000629-78-7/38 4 Heptadecane 240 C17H36 000629-78 38 Abundance Scan 4443 (29.184 min): 9570.D (-4430) (-) m/z 57.20 100.00% 43 5 7 71 85

wwa""W,yl 5000 105 141 124 164 183

mfe-> 0 108 i ■ ■' ‘I 20 40 60 80 |L i ■1 1 I ■ 1 I ' ' ’’ i i - ■ ■ ■ i ■ ■ ■ ■ i 100 120 140 160 180 200 220 240 260 280 300 I " 1 11 ' 1 1 rl '■''‘■'I 1 28.80 29.00 29.20 29.40 29.60 m/z 43.15 96.24% Abundance 43 57 #109656: Heneicosane WWWWNMwAM,, 71 5000 85 28 80 29.00 29.20 29.40 29.60 m/z 71.10 95.37% I, . 99 113127 141 155 169 183 197 211 225 239 253 267 281 296 m/z-> Abundance — 0 Ir TTpm** 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 MhMiphy, #112329: Octadecane 43 57

71 28.80 29.00 29.20 29.40 29.60 5000 m/z 85.10 83.94% 85

0 — I 29 113 127 141 155-169183197211225239 254 IT119IIIPIPTPTT wapowuo/yu. m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #112322: Heptadecane 43 57 28.80 29.00 29.20 29.40 29.60 m/z 97.10 67.44% 5000 29 71 85 Mabwup/W 99

n/z-> 0 u । 113127141155169183197211 240 — - mpmnt 1 ■ ■ I ■1 ■ ■ i ■ ■'1 i ■1 ■ ■ i ■ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 28.80 29.00 29.20 29.40 29.60

9570.D 050102.M Mon May 13 11:46:46 2002 Page 13

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