GCMS analysis results for sample AE09571, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050902\9570.D Vial: 7 Acq On 9 May 2002 8:10 pm Operator: Mclean Sample 5/8 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 8 Triallylphosphine Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T. 29.43 1.44 ug/L 2503820 Chrysene-dl2 30.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Triallylphosphine 154 C9H15P 016523-89-0 12 2 5,10-Tetradecanedione 226 C14H2602 029210-62-610 3 3-Oxa-l-azabicyclo[3.2.0]heptan-... 169 C9H15N02 086046-39-19 4 3-Piperidinone, 1-methyl-113 C6H11NO 005519-50-6 9 Abundance Scan 4485 (29.431 min): 9570.D (-4474) (-) m/z 57.10 100.00% 57 85

5000 41 70 113 MWMAu 99 126 141 153 165 183

, 207. —l —l .l, i II, J I 193 29.00 29.20 29.40 29.60 29.80 0■ i ' ■ ■ ■ i ' ' 1 1 L • m/ z 85.10 94.49% m/z- > 20 40 60 80 100 120 140 160 180 200 220 Abundance 41 71 85 #34087: Triallylphosphine awMuswlooh,, 126 5000 57 113 29.00 29.20 29.40 29.60 29.80 100 153 27 m/z 84.10 63.23%

miz-> Abundance ol । All, il]n I". 20 40 60 57 4ll 80

85 1——— - 100 120 139

140 #34297: 5,10-Tetradecanedione 160 180 200 220 wyMHalaiim 29.00 29.20 29.40 29.60 29.80 5000 41 126 m/z 113.10 54.00%

n/z-> 0-1 ' ' ' ' 1 Abundance 20 40 67 I 100 111I i । । "F| i |l) । l I, , Hi ‘ , J 4I—9 60 80 100 120 , 141151 169 , 198208 226 —1 140 ——9p — 160 m*m—m — 184 —92——m— 180 200 220 #33912:3-Oxa-1-azabicyclo[3.2.0]heptan-4-one, 2-(1,1-dime... Vy #MWh*sh NN 84 29.00 29.20 29.40 29.60 29.80 m/z 70.05 53.46%|

5000

28 41 56 112 WMMyA"“yMyPypwk .. 69 0 — 9111 98 ‘ '"I 1 ■' , 126. 141 154 199.................. m/z—> 20 40 60 80 100 120 140 160 180 200 220 29.00 29.20 29.40 29.60 29.80

9570.D 050102.M Mon May 13 11:46:47 2002 Page 14

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