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GCMS analysis report, sample AE02339, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010610–000010630

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data 'File C:\MSDCHEM\l\DATA\030402\2339.D Vial: 11 •Acq On 4 Mar 2002 6:27 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 9 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

27.56 0.92 ug/L 448511 Chrysene-dl2 30.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72012Sil2 018919-94-3 80 2 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57N03S12 000000-00-0 80 3 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN205 109007-87-6 43 4 lH-Purin-6-amine, [(2-fluOrophen... 243 C12H10FN5 074421-44-6 38 Abundance Scan 2699 (27.557 mln): 2339.D (-) m/z 73.05 100.00% 73

5000 147 221 281 355 —r. n .... 429 27.20 27.40 27.60 27.80 m/z 147.10 45.46% 0 — T* TTH —H AHH ■ i"1 • I ■ • • • i ■ ■ ■ ■ i1 ■' • i ■ • miz—> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclod > 73 355

5000 147 221 281 • i • ‘ • i • TE - 'I1' 27.20 27.40 27.60 27.80 m/z 221.10 35.36% 415 . . a | >1 r mi, AA . । . li'Jili i i | i > i i 11 । । 11 । 1 i । । > ii i | i i 0 •n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIE: 73 11 “ ' ■ r'r ••।••••।• 27.20 27.40 27.60 27.80 5000 m/z 355.00 23.84% 174 129 337 i 111 211 । -+4III 429 0-... AMMHhtmmh/1 |S‘lL (T> 11 |VI l I | I I I I | > I I I | I I m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic... 73 _mmmmm 27.20 27.40 27.60 27.80 m/z 281.00 20.87%

147 221 5000 355 281 429

26 111 503

m/z-> 0 ~444ua,183/ —417441 '• m1"11 i1 p • lP r14 577 ...................................... 50 100 150 200 250 300 350 400 450 500 550 600 650 652 ‘11 Mtee TTPIprufr ■ ‘ i ■ ■ ■ • i ■ 27.20 27.40 27.60 27.80

2339.D 5080302.M Mon Mar 18 08:32:47 2002 Page 11

NYC-WTC_000010625

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NYC-WTC_000010625Source: NYC Law Department, mirrored locally

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