NYC 9/11 Public Portal Document
Library Search Compound Report
Data 'File C:\MSDCHEM\l\DATA\030402\2339.D Vial: 11
•Acq On 4 Mar 2002 6:27 pm Operator: McLean
Sample 1/31 Inst : Instrumen
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
Peak Number 9 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
27.56 0.92 ug/L 448511 Chrysene-dl2 30.34
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72012Sil2 018919-94-3 80
2 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57N03S12 000000-00-0 80
3 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN205 109007-87-6 43
4 lH-Purin-6-amine, [(2-fluOrophen... 243 C12H10FN5 074421-44-6 38
Abundance Scan 2699 (27.557 mln): 2339.D (-) m/z 73.05 100.00%
73
5000 147
221
281 355 —r. n ....
429 27.20 27.40 27.60 27.80
m/z 147.10 45.46%
0 — T* TTH —H AHH ■ i"1 • I ■ • • • i ■ ■ ■ ■ i1 ■' • i ■ •
miz—> 50 100 150 200 250 300 350 400 450 500 550 600 650
Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclod >
73
355
5000 147 221 281
• i • ‘ • i • TE - 'I1'
27.20 27.40 27.60 27.80
m/z 221.10 35.36%
415
. . a | >1 r mi, AA . । . li'Jili i i | i > i i 11 । । 11 । 1 i । । > ii i | i i
0
•n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650
Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIE:
73
11 “ ' ■ r'r ••।••••।•
27.20 27.40 27.60 27.80
5000 m/z 355.00 23.84%
174
129 337
i 111 211 ।
-+4III 429
0-... AMMHhtmmh/1 |S‘lL (T> 11 |VI l I | I I I I | > I I I | I I
m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650
Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic...
73 _mmmmm
27.20 27.40 27.60 27.80
m/z 281.00 20.87%
147 221
5000 355
281 429
26 111 503
m/z->
0 ~444ua,183/ —417441 '• m1"11 i1 p • lP r14 577
......................................
50 100 150 200 250 300 350 400 450 500 550 600 650
652
‘11 Mtee TTPIprufr ■ ‘ i ■ ■ ■ • i ■
27.20 27.40 27.60 27.80
2339.D 5080302.M Mon Mar 18 08:32:47 2002 Page 11
NYC-WTC_000010625
OCR can misread numbers and units. Confirm readings against the page image before using them.