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GCMS method 508 scan data for WTC samples, March 2002

Machine-extracted title · confidence 90%

Instrument data file containing chromatographic scans and compound identification for environmental samples analyzed in March 2002.

NYC-WTC_000037884–000037905

Folder label: “GCMS X 2/20/02 A 3/20/02

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Scanned page image, NYC-WTC_000037903
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031902\3800.D Vial: 10 Acq On : 19 Mar 2002 7:02 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 15 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

34.95 0.97 ug/L 261445 Perylene-dl2 34.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72O12S112 018919-94-3 86 2 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 47 3 lH-Purin-6-amine, [(2-fluorophen... 243 C12H10FN5 074421-44-6 37 4 3-Isopropoxy-1,1,1,7,7,7-hexamet... 576 C18H5207S17 071579-69-6 28 Abundance Scan 3514 (34.949 mln): 3800.D (-) m/z 73.05 100.00% 73

147 221 5000 281 355 ‘I i ■ ‘ ■ i • • • ■ i 429 34.60 34.80 35.00 35.20 m/z 147.10 67.01% m/z-> 0 mm "■■I 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cycled ) 73 355

5000 147 221 281 AT 1 ‘ ’ 1 34.60 34.80 35.00 35.20 m/z 221.10 55.05% 415 0 TTTI np— trh — -Tppe mlz—> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic ... 73 ... L. 34.60 34.80 35.00 35.20 TAt 147 221 m/z 281.00 29.80% 5000 355 281 429 26 503

m/z-> 0 0 ulla4lllu Hmmmp | 577

50 100 150 200 250 300 350 400 450 500 550 600 650 700 652

Abundance #177443: 1H-Purin-6-amine, [(2-fluoropheny!)methyl]- (CAS) nhsahan TT 73 34.60 34.80 35'00 35.20 m/z 355.00 23.85% 147 28 221 5000 355 281 429 503

m/z—> oM 0 lalshauncl alll nntmm .. 563607653 703 50 100 150 200 250 300 350 400 450 500 550 600 650 700 ..... LA... 34.60 34.80 35.00 35.20

3800.D 5080302.M Thu Mar 21 11:42:37 2002 Page 17 • NYC-WTC_000037903

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NYC-WTC_000037903Source: NYC Law Department, mirrored locally

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