Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03801 conducted on March 22, 2002.
NYC-WTC_000037906–000037926Folder label: “GCMS X 2/20/02 A 3/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\031902\3801.D Vial: 11 Acq On : 19 Mar 2002 7:51 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L
Peak Number 7 1,1,1,5,7,7,7-Heptamethyl-3... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.39 1.04 ug/L 525760 Phenanthrene-dl0 22.50
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 50 2 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 50 3 Iron, monocarbonyl-(1,3-butadien— 438 C21H22FeN2O5 109007-87-6 39 4 lH-Purin-6-amine, [ (2-fluorophen... 243 C12H10FN5 074421-44-6 32 Abundance Scan 2129 (22.387 min): 3801 .D (-) m/z 73.10 100.00% 73
5000 147 221 .... — . — 281 355 429 22 00 22.20 22.40 22.60 22.80
m/z-> 0-TH T)**r - TIfu — l 50 100 150 200 250 300 350 400 450 500 550 600 650 m/z 147.10 28.00%
Abundance #352530:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy. .. 73
147 5000 267 355 A 22.00 22.20 22.40 22.60 22.80 429 207 m/z 221.10 22.28%
m/z—> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DI(: 73
22.00 22.20 22.40 22.60 22.80 5000 m/z 355.10 11.22% 174 129 337 221 281 , 429
m/z-> ull 0-I.,,, ---------- ............ .390.44 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbonyl-(1,3-butadfene-1,4-dicarbonic... - 73 ■ i ■ • > ■ i ■ • 22.00 22.20 22.40 22.60 22.80 m/z 429.10 10.41%
147 221 5000 355 281 429
26 111 503
m/z—> 0J -ulaauas 183 — 1 # =4 n — t 3171,.... ................. 50 100 150 200 250 300 350 400 450 500 550 600 650 577 652 T T 22.00 22.20 22.40 22.60 22.80
3801.D 5080302.M Thu Mar 21 11:43:51 2002 Page 9
NYC-WTC_000037919
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NYC-WTC_000037948
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03804 conducted on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037884
Instrument data file containing chromatographic scans and compound identification for environmental samples analyzed in March 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037870
Laboratory report listing concentrations of volatile organic compounds in sample AE03799 analyzed on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037964
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03805 conducted on March 22, 2002.
Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010610
Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012129
Laboratory report for GC/MS re-injection of sample 1639 using Method 508 scan on March 20-21, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010537
Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010659
Laboratory report detailing gas chromatography-mass spectrometry analysis of environmental sample AE02381 conducted on March 22, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010585
Laboratory analysis report for sample AE02338 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010488
Laboratory analysis report for sample AE02334 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010513
Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011347
Laboratory report documenting GCMS blank analysis of environmental sample AE03265 conducted on March 25, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000037819
Department of Environmental Protection site log sheet for the World Trade Center area covering February and March 2002.
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NYC-WTC_000037820
Log sheet recording sample preparation details including drip rates and pH for GCMS analysis in March 2002.
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Laboratory report listing quantitative concentrations of volatile organic compounds in sample AE00364 analyzed on March 21, 2002.
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NYC-WTC_000037829
Reference data report for GCMS analysis of sample AE00364 showing peak identification and response values from March 21, 2002.
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Laboratory report documenting GCMS analysis of a method blank for sample AE00364 to verify analytical system cleanliness.
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