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GCMS analysis report, sample AE02339, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010610–000010630

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\030402\2339.D Vial: 11 Acq On 4 Mar 2002 6:27 pm Operator: McLean Sample 1/31 Inst ; Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 6 1,1,1,5,7,7,7-Heptamethyl-3... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.41 1.36 ug/L 672611 Phenanthrene -dl0 22.52

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,1,1,5,7,7,7-Heptamethyl-3,3-bi. . . 444 C13H4005Si6 038147-00-1 50 2 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57N03S12 000000-00-0 50 3 F2A 13,14-H2 ME ESTER 3TMS 586 C30H6205S13 000000-00-0 42 4 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN205 109007-87-6 40 Abundance Scan 2132 (22.414 mln): 2339.D (-) m/z 73.10 100.00%| 73

5000 147 221 T i ‘ ' ri T 281 355 429 22.00 22.20 22.40 22.60 22.80 ‘ I ■ ■■ Pin nifm M Tr+43541 45 117 117 251 191 m/z 147.10 29.39% m/z—> 0-1 0 50 100 150 200 250 > 300 350 400 450 500 Abundance #352530:1,1,1,5,7,7,7-HeptamethyI-3,3-bis(trimethylsiloxy... 73

147 5000 267 T Tt‘ 355 429 22.00 22.20 22.40 22.60 22.80 207 m/z 221.10 21.91%

----- 01 >.. ■ । ‘ i ■ * -p-r-r-r-p-r • l • • ■ • | ■ m/z—> 0 50 100 150 200 250 300 350 400 450 500 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIE: 73

22.00 22.20 22.40 22.60 22.80 5000 m/z 355.10 11.76% 174 129 337 221

/z—> 0 01 4dl --—mpe 369 I 50 100 150 200 250 300 350 400 450 500 , 429

Abundance #380705: F2A 13.14-H2 ME ESTER 3TMS ............................................ 73 22.00 22.2022.40 22.60 22.80 m/z 429.10 11.67%

5000 173 224 259 129 320 355 429 /z—> 14 OTT* ,49144 44 4 4 0 21424LL, 500 50 100 150 200 250 300 350 400 450 500 22.00 22.20 22.40 22.60 22.80

2339.D 5080302.M Mon Mar 18 08:32:44 2002 Page 8

NYC-WTC_000010622

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NYC-WTC_000010622Source: NYC Law Department, mirrored locally

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