NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\l\DATA\030402\2339.D Vial: 11
Acq On 4 Mar 2002 6:27 pm Operator: McLean
Sample 1/31 Inst ; Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
Peak Number 6 1,1,1,5,7,7,7-Heptamethyl-3... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.41 1.36 ug/L 672611 Phenanthrene -dl0 22.52
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethyl-3,3-bi. . . 444 C13H4005Si6 038147-00-1 50
2 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57N03S12 000000-00-0 50
3 F2A 13,14-H2 ME ESTER 3TMS 586 C30H6205S13 000000-00-0 42
4 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN205 109007-87-6 40
Abundance Scan 2132 (22.414 mln): 2339.D (-) m/z 73.10 100.00%|
73
5000
147
221 T i ‘ ' ri T
281 355 429 22.00 22.20 22.40 22.60 22.80
‘ I ■ ■■ Pin nifm M Tr+43541
45 117
117
251 191 m/z 147.10 29.39%
m/z—>
0-1
0 50 100 150 200 250 > 300 350 400 450 500
Abundance #352530:1,1,1,5,7,7,7-HeptamethyI-3,3-bis(trimethylsiloxy...
73
147
5000 267 T Tt‘
355 429 22.00 22.20 22.40 22.60 22.80
207 m/z 221.10 21.91%
-----
01 >.. ■ । ‘ i ■ * -p-r-r-r-p-r • l • • ■ • | ■
m/z—> 0 50 100 150 200 250 300 350 400 450 500
Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIE:
73
22.00 22.20 22.40 22.60 22.80
5000 m/z 355.10 11.76%
174
129 337
221
/z—> 0
01 4dl --—mpe
369 I
50 100 150 200 250 300 350 400 450 500
, 429
Abundance #380705: F2A 13.14-H2 ME ESTER 3TMS ............................................
73
22.00 22.2022.40 22.60 22.80
m/z 429.10 11.67%
5000
173 224 259
129 320 355 429
/z—>
14
OTT* ,49144 44 4 4
0
21424LL, 500
50 100 150 200 250 300 350 400 450 500 22.00 22.20 22.40 22.60 22.80
2339.D 5080302.M Mon Mar 18 08:32:44 2002 Page 8
NYC-WTC_000010622
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