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GCMS analysis report, sample AE02338, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02338 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010585–000010609

Folder label: “GCMS X 1/31/02 A 3/4/02

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Scanned page image, NYC-WTC_000010600
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\03 04 02\2 33 8.D Vial: 10 Acq On 4 Mar 2002 5:38 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 9 BISTRIMETHYLSILYL N-ACETYL ... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.41 1.92 ug/L 932276 Phenanthrene - dl 0 22.52

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 53 2 l,l,l,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H4005Si6 038147-00-1 42 3 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 42 4 SILICONE POLYMER 458 C14H4205Si6 000000-00-0 40 Abundance Scan 2132 (22.413 min): 2338.D (-) m/z 73.10 100.00% 73

5000 147 221 429 22*00 22.20 22.40 22.60 22.80 281 355 m/z 147.10 29.28% 0 TIh p*r — m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPH1NGA-4,11-Dlf l 73

5000 174 22.00 22.2022.40 22.60 22.80 129 337 m/z 221.10 20.49% 221 281 . 429

•n/z-> 0- 44 rrr।M.390 . I 1*1T, ।।।। . 50 100 150 200 250 300 350 400 450 500 550 600 650 . Abundance #352530:1,1,1,5,7,7,7-Heptaniethyl-3.3-bis(Wmethylsiloxy ... 73 .................. ............... 147 22.00 22.2022.40 22.60 22.80 267 m/z 429.10 12.15% 5000 355 429 207

0- T I'“’I‘'•u T i' * *' 1 TT I • • *' I TTTT miz-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocart>onyl-(1,3-butadiene-1,4-dicarbonic ... 73 22.00 22'20 22*40 22.60 22.80 m/z 355.00 11.26%

147 221 5000 355 281 429 26 144 503

m/z—> 0 444,834.4HU u 1 ■■ m etempingt .-rrr rffrr 50 100 150 200 250 300 350 400 450 500 550 600 650 1 577 652 T T T T 22.00 22.20 22.40 22.60 22.80

2338.D 5080302.M Mon Mar 18 08:32:18 2002 Page 11

NYC-WTC_000010600

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NYC-WTC_000010600Source: NYC Law Department, mirrored locally

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