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GCMS analysis report, sample AE02338, March 22, 2002

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Laboratory analysis report for sample AE02338 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010585–000010609

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\030402\2338.D Vial: 10 Acq On : 4 Mar 2002 5:38 pm Operator: McLean Sample : 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 8 Benzoic acid, 2,4-bis[(trim... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 20.31 2.42 ug/L 1157150 Acenaphthene-dl0 18.17 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, 2,4-bis[(trimethyl... 370 C16H30O4Si3 010586-16-0 38 2 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 35 3 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 35 4 n-Nonadecanoic acid, pentamethyl... 428 C24H52O2Si2 000000-00-0 35 Abundance Scan 1900 (20.309 min): 2338.D (-) m/z 73.10 100.00%] 73

5000 147 355 221 281 20.00 20.20 20.40 20.60 45 327 401 TITT — — - g 117P." 4 191191, rih 249 ( | m/z 355.10 31.00%l 01 miz-> 50 100 150 200 250 300 350 400 Abundance #313243: Benzoic acid, 2,4-bis[(trimethyisilyl)oxy]-, trim... 73

5000 355 20.00 20.20 20.40 20.60 45 m/z 147.10 27.54%

0- 16 . 105 133,163 193,223 251 21 —I4r **9 321 IT • 1 ■ n/z-> 50 100 150 200 250 300 350 400 Abundance #331718: Phenethylamine, N-methyl-beta.,3,4-tris(trimethy... 73 TPPTI T 1 • * ■ ■ 1 20.00 20.20 20.40 20.60 5000 m/z 221.10 24.55 355

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। 116 147 193 220 267 294 384 0- T1 ‘ *r sdssssruarihri-vi miz-> 50 100 150 200 250 300 350 400 Abundance #322218: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 73 147 20*66 20'20 2040 20.60 7 m/z 281.10 15.29 281 5000

369 45 207 20 m/z—> 0 —1 50 117 remandirr 177 1 249 * 310 341 | • i ■ ■ ■ ■ i • ’ ‘ ■ i ■ ■ ■ ■ i ■ • • ■ i ■ 100 150 200 250 300 350 400 20.00 20.20 20.40 20.60

2338.D 5080302'.M Mon Mar 18 08:32:17 2002 Page 10

NYC-WTC_000010599

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NYC-WTC_000010599Source: NYC Law Department, mirrored locally

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