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GCMS analysis report for sample AE02335, March 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010513–000010536

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

.- Data'File : C:\MSDCHEM\1\DATA\030402\2334.D Vial: 14 Acq On : 4 Mar 2002 8:54 pm Operator: McLean Sample : 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 7 Phenethylamine, N-methyl-.b... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

20.31 2.71 ug/L 1261450 Acenaphthene-dl0 18.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3S13 010538-85-9 35 2 n-Nonadecanoic acid, pentamethyl... 428 C24H5202S12 000000-00-0 35 3 Benzoic acid, 2,6-bis [ (trimethyl... 370 C16H3004Si3 003782-85-2 32 4 Benzoic acid, 2,5-bis(trimethyls... 370 C16H30O4Si3 003618-20-0 27 Abundance Scan 1900 (20.309 min): 2334.D (-) m/z 73.10 100.00% 73

5000 147 355 221 281 20.00 20.20 20.40 20.60 45 .. 117 191 , 249 , 327 401 m/z 355.10 30.76% 0— 1-P* **4 ■ ■ r 14 Fi" r 144 rur- m/z-> 50 100 150 200 250 300 350 400 Abundance #331718: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... 73

5000 355 20.00 20.20 20.40 20.60 1 44 m/z 147.10 29.02%

Ji , । 0 , m+4h, 116 147 I-.-) , ■ i 1931 •220 267 294 > i ■ -i r 1* r "i : . 384 miz-> 50 100 150 200 250 300 350 400 Abundance #346318: n-Nonadecanoic acid, pentamethyldisilyl ester 43 73 355

T T T T 1 20.00 20.20 20.40 20.60 147 m/z 221.10 24.53% 5000 413 203

m/z-> 0- J 44 50 100 195 117

150 200 245 ----- 250 295 325 300 350 400 Abundance #313257: Benzoic add. 2,6-bis[(trimethylsilyl)oxy]-, trim... 73 355 ■n-p-m-j-T mPPPPT 20.00 20.20 20.40 20.60 m/z 281.00 16.52%

5000

147 267

m/z-> 44 195- 01 • i ' r 50 - 100 +247,+,313 119 179.207 150 200 250 300 350 ■ > i% t । । 400 ■ 20.00 20.20 20.40 20.60 T

2334.D 5080302.M Mon Mar 18 08:30:59 2002 Page 9

NYC-WTC_000010526

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NYC-WTC_000010526Source: NYC Law Department, mirrored locally

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