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GCMS blank results for sample AE03799, March 22, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03799 to verify analytical system cleanliness.

NYC-WTC_000037848–000037869

Folder label: “GCMS X 2/20/02 A 3/20/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\031902\220LB.D Vial: 8 Acq On : 19 Mar 2002 5:24 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 7 Phenethylamine, N-methyl -.b... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 20.28 3.02 ug/L 1730380 Acenaphthene-d10 18.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 Phenethylamine, N-methyl -.beta., ... 399 C18H37NO3Si3 010538-85-9 35 2 n-Nonadecanoic acid, pentamethyl. .. 428 C24H52O2Si2 000000-00-0 35 3 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 25 4 Benzeneacetic acid. .aluha..3.4-. .. 472 C20H40O5Si4 037148-65-5 25 bundance Scan 1897 (20.282 min): 220LB.D (-) m/z 73.10 100.00

5000 147 355 221 281 401 20.00 20.20 20.40 20.60 45 117 191 249 327 m/z 355.10 33.34 0 -> 50 100 150 200 250 300 350 400 bundance #331718: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy...

5000 355 20.00 20.20 20.40 20.60 44 m/z 147.10 28.96

116 147 193 220 267294 384 0 n/z-> 50 100 150 200 250 300 350 400 undance #346318: n-Nonadecanoic acid, pentamethyidisilyl ester 443 73 3

20.00 20.20 20.40 20.60 147 m/z 221.10 24.17 5000 413 203 97 0 245 295 325 -> 50 100 150 200 250 300 350 400 thundance #357156: Noradrenaline tetraTMS 20.00 20.20 20.40 20.60 m/z 281.10 15.71

5000 355 102

45 147 442 0 Ii . -> 50 100 150 200 250 300 - 350 400 20.00 20.20 20.40 20.60

'17 ATD r% GAOA)A7 tut TA.. 1ut..... - 7 '1

NYC-WTC 000037860

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NYC-WTC_000037860Source: NYC Law Department, mirrored locally

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