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GCMS blank results for sample AE03799, March 22, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03799 to verify analytical system cleanliness.

NYC-WTC_000037848–000037869

Folder label: “GCMS X 2/20/02 A 3/20/02

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Scanned page image, NYC-WTC_000037861
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

9 Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031902\220LB.D Vial: 8 Acq On : 19 Mar 2002 5:24 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 8 BISTRIMETHYLSILYL N-ACETYL ... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. ------------------------- -7------------------------------------------ 22.39 2.29 ug/L 1323680 Phenanthrene-d10 22.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 43 2 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 43 3 F2A 13,14-H2 ME ESTER 3TMS 586 C30H62O5Si3 000000-00-0 42 4 1,1,1,5.7.7.7-Hebtamethvl-3.3-bi... 444 C13H40O5Si6 038147-00-1 40 undance Scan 2129(22.387 min): 220LB.D (-) m/z 73.10 100.00

5000 147 221 281 355 429 22.00 22.20 22.40 22.60 22.80 m/z 147.10 28.30 0 ntz-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 undance#370710: BISTRIMETHYLSILYL NACETYL EICOSASPHINGA-4,11-DI

5000 174 22.00 22.20 22.40 22.60 22.80 129 337 m/z 221.10 22.23 221 281 429 380 0 rilz-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 undance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic ...

22.00 22.20 22.40 22.60 22.80 147 221 5000 m/z 355.10 11.76 355 281 429 26 503 111 1 577 31 652 0 i/z-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 bundance #380705: F2A 13.14-112 ME ESTER 3TMS 22.00 22.20 22.40 22.60 22.80 m/z 429.10 11.63

5000 173 224 1 320 429 14 500 0 n/z-> 0 50 100 150 200 250 300 350 400 450.500 550 600 650 22.00 22.20 22.40 22.60 22.80

' 5'ATD T CAOA)An V ml.... sa....., n1 fi n rn an nnnn

NYC-WTC 000037861

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NYC-WTC_000037861Source: NYC Law Department, mirrored locally

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