NYC-WTC_000037948
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03804 conducted on March 22, 2002.
Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 14 pages
GCMS analysis results for sample AE03805, March 22, 2002
Machine-extracted title · confidence 100%Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03805 conducted on March 22, 2002.
NYC-WTC_000037964–000037977Folder label: “GCMS X 2/20/02 A 3/20/02”
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OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
. « Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\031902\3805.D Vial; 15 Acq On : 19 Mar 2002 11:07 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L
Peak Number 6 BISTRIMETHYLSILYL N-ACETYL ... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.39 0.61 ug/L 296071 Phenanthrene-dl0 22.50
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 59 2 1,1,1,5,7,7, 7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 42 3 F2A 13,14-H2 ME ESTER 3TMS 586 C30H62O5Si3 000000-00-0 40 4 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 38 Abundance Scan 2129 (22.387 mln): 3805.D (-) m/z 73.10 100.00% 73
5000 147 221 I'11' I 1’1 281 355 429 22.00 22.20 22.40 22.60 22.80
m/z—> 0T — —fo 1911 0 50 117 100 150 200 2511,22511 —401 1——— 250 300 350 400 450 500 m/z 147.10 30.69%
Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIE 73
.......... — 5000 174 22.00 22.20 22.40 22.60 22.80 129 337 m/z 221.10 20.83% 221 281 — miz-> 0^ 0 340.1,309.809—44— 50 100 150 200 250 300 350 400 450 500 Abundance #352530; 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy... 70 ........ .............. 11 ■ ■ ■ ■ 111 147 22.00 22.20 22.40 22.60 22.80 267 m/z 429.10 10.73% 5000 355 429 207
0i 1 1 ’I ■ ■ i ‘ 11 ■ i ■ ‘ TIIt m/z—> i0 50 100 150 200 250 300 350 400450 500 Abundance #380705: F2A 13,14-H2 ME ESTER 3TMS 73 T’tttr’rr TTTT 22.00 22.20 22.40 22.60 22.80 m/z 355.10 10.66%
5000 173 224 259 129 320 429
m/z—> 0-T *i 14 ,491144111,141423524, 1 500, 22.00 22.20 22.40 22.60 22.80 0 50 100 150 200 250 300 350 400 450 500
3805.D 5080302.M Thu Mar 21 11:49:09 2002 Page 8 NYC-WTC_000037976
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NYC-WTC_000037976Source: NYC Law Department, mirrored locally
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