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← Document results/DEP Box 14/GCMS X 2/14/02 A 3/2/02 - 3/20/02
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GCMS blank analysis results for sample AE03265, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS blank analysis of environmental sample AE03265 conducted on March 25, 2002.

NYC-WTC_000011347–000011364

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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Scanned page image, NYC-WTC_000011361
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NYC 9/11 Public Portal Document

Library Search Compound Report • Data File : C:\MSDCHEM\1\DATA\031902\0214LB.D Vial: 33 Acq On : 21 Mar 2002 5:58 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 8 BISTRIMETHYLSILYL N-ACETYL .. Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

25.98 0.53 ug/L 640154 Phenanthrene-dl0 22.51

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 59 2 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 40 3 3-Isopropoxy-1,1,1,7,7,7-hexamet... 576 C18H5207Si7 071579-69-6 37 4 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 . 003555-47-3 37 Abundance Scan 2525 (25.978 min): 0214LB.D (-) m/z 73.10 100.00% 73

5000 147 221 355 281 ■ i1'1 '"i reer PPP ■■■'!' 25.60 25.80 26.00 26.20 325 ’Pih '' 1911—— A*** 139942 .... , m/z 147.10 39.60% 0 T’tr 1’1 1117. m/z—> 50 100 150 200 250 300 350 400 450 500 550 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-Dlf: 73

5000 TT T 1‘ T TT 174 25.60 25.80 26.00 26.20 129 337 m/z 221.10 29.96% 221 281

miz-> O+ 42144 50 100 150 200 250 300 350 400 450 500 550 . 429 ....... .

Abundance #361625: Benzeneacetic acid, .alpha.,3,4-tris((trimethyisi... 73

25.60 25.80 26.00 26.20 5000 355 m/z 355.00 29.85%

105 I 147 193 251 295325 429 472 0+ 29 ■»■ I * A»< i ATYTTPTT i ■ • 1 • i '■ ■ ■ ■ i ■ ■ ■ • i ■ ■

m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #379639:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3.5,5-tris(tr... ...... I \...... 73 25.60 25*80 26.66 26.20 ~ m/z 281.10 20.64%

5000 147 43 221 281 29- .I | 327 1 519 561 0- oh’ 119*mm9mmmmm9*mtmmmmpke m/z—> 50 100 150 200 250 300 350 400 450 500 550 25.60 25.80 26.00 26.20 1

0214LB.D 5080302.M Mon Mar 25 08:59:26 2002 Page 10

NYC-WTC_000011361

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NYC-WTC_000011361Source: NYC Law Department, mirrored locally

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