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GCMS analysis results for sample AE02381, March 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of environmental sample AE02381 conducted on March 22, 2002.

NYC-WTC_000010659–000010676

Folder label: “GCMS X 1/31/02 A 3/4/02

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Scanned page image, NYC-WTC_000010670
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\030402\2381.D Vial: 16 Acq On 4 Mar 2002 10:32 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 5 BISTRIMETHYLSILYL N-ACETYL ... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.41 0.79 ug/L 361098 Phenanthrene-d10 22.52

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NOBSi 000000-00-0 47 2 F2A 13,14-H2 ME ESTER 3TMS 586 C30H6205Si3 000000-00-0 42 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H400SSi 038147-00-1 40 4 morphin silyliert 429 C23H35N03S12 000000-00-0 35 Abundance Scan 2132 (22.414 min): 2381 .D (-) I /m/z 73.10 100.00% 73

5000 147 221 1****1*********1** 281 355 429 22.00 22.20 22.40 22.60 22.80 — -117— 191251432411 45 m/z 147.10 31.30% m/z—> 0T 0 50 100 150 200 250 300 350 400 450 500 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4.11-DIH 73

5000 174 T T A 113 22.00 22.20 22.40 22.60 22.80 . 129 337 m/z 221.10 24.95% 221

0T—T jaal—— I 281 , 429

m/z—> 0 A9,,399.4,a?.,'-.!.,....,. 50 100 150 200 250 300 350 400 450 500 Abundance #380705: F2A 13,14-H2 ME ESTER 3TMS 73 T i ■1111 T T 22.00 22.20 22.40 22.60 22.80 5000 m/z 355.00 10.95% 173 224 259 129 320 . I w 429 0 PTtH 14 914al——mmepmt ................... 500 291 . । 384 i [ m/z-> ।0 50 100 150 200 250 300 350 400 450 500 Abundance #352530:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy... 73 22.00 22.20 22.40 22.60 22.80 m/z 429.10 10.35% 147 5000 267 355 429 207

OTTT m/z—> 0 50 100 150 200 250 300 350 400 450 500 T 1t T T 22.00 22.20 22.40 22.60 22.80

2381.D 5080302.M Mon Mar 18 08:33:23 2002 Page 7

NYC-WTC_000010670

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NYC-WTC_000010670Source: NYC Law Department, mirrored locally

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