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GCMS analysis results for sample AE02381, March 2002

Machine-extracted title · confidence 100%

Laboratory report detailing gas chromatography-mass spectrometry analysis of environmental sample AE02381 conducted on March 22, 2002.

NYC-WTC_000010659–000010676

Folder label: “GCMS X 1/31/02 A 3/4/02

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\030402\2381.D Vial: 16 Acq On : 4 Mar 2002 10:32 pm Operator: McLean Sample : 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

20.31 1.02 ug/L 463608 Acenaphthene-dl0 18.16

Hit# of 5 Tentative ID MW Mol Form CAS# Qual 1 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72012 il2 018919-94-3 56 2 Benzeneacetic acid, .alpha., 3,4-. . . 472 C20H40O5SJ.4 037148-65-5 40 3 2-TRIMETHYLSILYLAMINO-l-TRIMETHY... 457 C20H43N0381 068595-65-3 35 4 Cyclopentasiloxane, decamethyl- 370 C10H30O5SJ 5/ 000541-02-6 35 Abundance 73 Scan 1900 (20.310 min): 2381 .D (-) m/z 73.10 100.00%

5000 147 355 221 > >).... 11 ( A 11 1111111 281 401 20.00 20.20 20.40 20.60 45 117 191, 249, I 3?7 0 — Pr -I* 1 i Pr A * m/z 355.10 28.96% m/z—> 50 100 150 200 250 300 350 ' 400 " 450 " 500 Abundance#391010: TETRACOSAMETHYLCYCLODODECASiLOXANE $$ Cyclod 73 355

5000 147 221 281 1' I " " 11 ’ PmPPP 20.00 20.20 20.40 20.60 m/z 147.10 27.86% 415 3251

m/z-> 45 0- TTT 50 —119—191. 2491 TTT1** 1′1 100 150 200 250 300 350 -4 385400. 450 500 Abundance #361625: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... 73

20.00 20.20 20.40 20.601 5000 355 m/z 221.10 22.81%

0 29— 105 147 193 237267295325 -r-ryr-r '■ i ***du‘u • ■ f •"I >i‘| > । 11 । 384 429457 1 r 1 I ' 1 ' 1 1 '' 1 1 1 I ' /z—> 50 100 150 200 250 300 350 400 450 500 Abundance #357157:2-TRIMETHYLSILYLAMINO-1-TRlMETHYLSILYLOXY-1-(3‘.4. 73 20.00 20.20 20.40 20.60117 m/z 281.10 17.79% 355

5000 102

45 147 . 486 179207 -- 251281 ----- 3255 382410 442 | 0 ■ . -14. 1*1m —fo*mPTTTI m/z—> 50 100 150 200 250 300 350 400 450 500 20.00 20.20 20.40 20.60

2381.D 5080302.M Mon Mar 18 08:33:22 2002 Page 6

NYC-WTC_000010669

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NYC-WTC_000010669Source: NYC Law Department, mirrored locally

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