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GCMS analysis report, sample AE02341, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02341 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010639–000010650

Folder label: “GCMS X 1/31/02 A 3/4/02

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Scanned page image, NYC-WTC_000010649
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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\030402\2341.D Vial: 13 Acq On : 4 Mar 2002 8:05 pm Operator: McLean Sample : 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method s C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 4 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

20.31 0.51 ug/L 235696 Acenaphthene- dl 0 18.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 TETRACOSAMETHYLCYCLODODECASILOXA... 888 C24H720129i12 018919-94-3 72 2 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005514 037148-65-5 37 3 Benzeneethanamine, N-[(pentafluo... 563 C24H34F5N03Si3 055429-13-5 35 4 n-Nonadecanoic acid, pentamethyl... 428 C24H5202Si2 000000-00-0 35 Abundance Scan 1900 (20.309 min): 2341.D (-) m/z 73.10 100.00%! 73

5000 147 355 221 281 401 20.00 20.20 20.40 20.60 117 0 —TH HTH 191 1 19/41.251, m/z 355.10 31.59 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cycled. > 73 355

5000 147 221 281 20.00 20.20 20.40 20.60 m/z 147.10 29.26%! 415

m/z-> 117. 01 1 'i1 ■ TTfm 191 - 325i 251 + ,395....)........ 50 100 150 200 250 300 350 400 450 500 550 Abundance #361626: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... 113

20.00 20.20 26'46 20.60 TT 5000 m/z 221.10 21.05? 355

147 i ri' "I 385 429458 ........... 41 251 295325 0- 11 . Mil ‘l . , 193 .117, rprujihi miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #378300: Benzeneethanamine, N-[(pentafluorophenyl)methylen... 73 T T i ■ ■ ■ ■ 1 • • ■' i 355 20.00 20.20 20.40 20.60 m/z 281.00 17.89

5000

117147177207 251281 4f, t 117147177207 0 । FI* A rfii Pi = 251281 rri r 11 _ fl's111__ । ri 11 ।S■ 386 429458 548 T’I T T T ‘I /z-> 50 100 150 200 250 300 350 400450500'550 ' 20.00 20.20 20.40 20.60

2341.D 5080302.M Mon Mar 18 08:33:07 2002 Page 6

NYC-WTC_000010649

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NYC-WTC_000010649Source: NYC Law Department, mirrored locally

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