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GCMS analysis report, sample AE02339, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010610–000010630

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\03 04 02\2 3 3 9. D Vial: 11 Acq On 4 Mar 2002 6:27 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 5 Benzeneethanamine, N-[(pent... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

20.31 1.71 ug/L 839604 Acenaphthene-dl0 18.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzeneethanamine, N-[(pentafluo... 563 C24H34F5NO3 055429-13-5 38 2 n-Nonadecanoic acid, pentamethyl... 428 C24H52O2Si2 000000-00-0 35 3 TETRACOSAMETHYLCYCLODODECASILOXA... 888 C24H72012Si 018919-94-3 32 4 Benzoic acid, 2,4-bis[(trimethyl... 370 C16H30O4Si3 010586-16-0 32 Abundance Scan 1900 (20.310 min): 2339.D (-) m/z 73.10 100.00%| 73

5000 355 147 221 281 401 20.00 20.20 26.46 26'66 ■n/z-> 0- — ‘ 8 117 *44+19421 191 . ...................... m/z 355.10 33.67% 50 100 150 200 250 300 350 400 450 500 550 Abundance #378300: Benzeneethanamine, N-K(pentaflucropheny!)methylen... 73 355

5000 "II T T 1 ■ ■ ■ ■ 1 20.00 20.20 20.40 20.60 m/z 147.10 28.70

miz-> 0- 50 4+ , 117147177207 11714717J207 251281 100 150 200 250 300 350 400 450 500 550 386 429458 543

Abundance #346318: n-Nonadecanoic acid, pentamethyldisilyl ester 43 73 355 TOTTI T T ‘I 20.00 20.20 20.40 20.60 147 m/z 221.10 22.52 5000 413 203

m/z—> 0 - 50 ul1 4 245.295325, / -Tmpp 100 150 200 250 300 350 400 450 500 550 Abundance*391010i TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclod > 355 20.00 20.20 20.46 20.60 1 m/z 281.00 16.18

5000 147 221 281

415

n/z—> 0 ■ •! 1 ■

50 117, I 191 ' ■1 1 100 251, + 1.385.,. 325 150 200 250 300 350 400 450 500 550 20.00 20.20 20*40 26'66 '

2339.D 5080302.M Mon Mar 18 08:32:43 2002 Page 7

NYC-WTC_000010621

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NYC-WTC_000010621Source: NYC Law Department, mirrored locally

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