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GCMS analysis results for sample AE03803, March 22, 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03803 conducted on March 22, 2002.

NYC-WTC_000037935–000037947

Folder label: “GCMS X 2/20/02 A 3/20/02

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Scanned page image, NYC-WTC_000037946
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\031902\3803.D Vial: 13 Acq On : 19 Mar 2002 9:29 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Benzeneacetic acid, .alpha.... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

20.28 0.53 ug/L 250663 Acenaphthene-dl0 18.13

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 35 2 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 35 3 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 35 4 3-Isopropoxy-1,1,1,7,7,7-hexamet... 576 C18H52O7Si7 071579-69-6 32 Abundance Scan 1897 (20.282 min): 3803.D (-) m/z 73.10 100.00% 73

5000 147 355 221 - — m 281 20.00 20.20 20.40 20.60 249, I 327 401 117 191,t 191. m/z 355.00 32.25% 0- — — ..r t.— —fr—T miz-> 50 100 150 200 250 300 350 ' 400 450 Abundance #361625: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... 73

5000 355 20.00 20.20 20.40 20.60 m/z 147.10 30.55% 147 47 105 I 193 237 267295 325 384 429457 0- TTTr TIguT*ImemenfeTeTTr r m/z-> 50 100 150 200 250 300 350 400 *480 Abundance #357156: Noradrenaline tetraTMS 73 - 20.00 20.20 20.40 20.60 m/z 221.10 23.51% 5000 355 102

45 147 442 0- | • • i ‘ m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313068: Cyclopentasiloxane, decamethyl- 73 1’1111 i 1,1 ’I 20.00 20.20 20.40 20.60 m/z 281.10 14.58% 355 267 5000

45 207 . 323, m/z—> 0 — 50 —I — —1 100 150 200 250 300 350 1 ■ 11 1 ■ ' ‘ 1 1 ‘ 400 450 • • i •11' i • 1——— 20.00 20.20 20.40 20.60

3803 n 5080302.M Thu Mar 21 11:46:14 2002 Page 7 NYC-WT C_000037946

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NYC-WTC_000037946Source: NYC Law Department, mirrored locally

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