NYC-WTC_000037870
Laboratory report listing concentrations of volatile organic compounds in sample AE03799 analyzed on March 22, 2002.
Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 13 pages
GCMS analysis results for sample AE03803, March 22, 2002
Machine-extracted title · confidence 100%Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03803 conducted on March 22, 2002.
NYC-WTC_000037935–000037947Folder label: “GCMS X 2/20/02 A 3/20/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\031902\3803.D Vial: 13 Acq On : 19 Mar 2002 9:29 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L
Peak Number 4 Trisiloxane, 1,1,1,5,5,5-he... Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
17.84 0.75 ug/L 353664 Ac enaphthene- dl 0 18.13
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H36O4Si5 003555-47-3 42 2 1,1,3,3,5,5,7,7,9,9,11,11-DODECA... 430 C12H38O5Si6 000000-00-0 40 3 Hexasiloxane, 1,1,3,3,5,5,7,7,9,... 430 C12H38O5Si6 000995-82-4 40 4 (trimethylsilyloxy) 2-(trimethy... 398 C18H27C104Si2 000000-00-0 28 Abundance Scan 1628 (17.843 min): 3803.D (-) m/z 73.10 100.00% 73
5000 147 281
327 T T 11 17.60 17.80 18.00 18.20 45 , 191 221 249. m/z-> 0- — 50 117 • ■ i ■ Ir 100 150 ' 1 1 f 200 1 1 1 1'1 250 300 Ll —383.415 350 400 m/z 147.10 37.35%
Abundance #322218: Trisiloxane. 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 73 147
281 5000 .A '1 11'11’I 1 • • • • 1 17.60 17.80 18.00 18.20 m/z 281.00 35.41% 369
m/z—> 0 + 45
50 117 —1 1 100 150 207 177 | Tfrr 200 249. — 250 310 341 1 I 1 1 1 ‘ I • 400 300 350 [ 1 1 I ' • Abundance#347007: 1,1,3,3,5,5,77,9,9,11,11-DODECAMETHYL-HEXASILOXANE 73 • ■ i' ■ ‘ ‘ i .s.,....... 17.6017.80 18.0018.20 5000 m/z 327.00 11.81% 281 207 133 341 4=
m/z-> 0- •45 — r 50 100 103 150 200 .253 1771123044 250 , 309, L 41 300 350 400 Abundance #347008: Hexasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11-dodecamethyl 73 1 • • ■ • 1 i • ■ • • 1 17.60 17.80 18.00 18.20 m/z 282.00 9.64%
5000 281 207 133 341
m/z—> 0 + 45 ।
50 -IP 1771—4 2302134 1 309 It 103 100 150 200 250 300 415 L I ■ ■ • • l • ‘ 350 400 1 • •'' i • ■ i • ■ • • i 17.60 17.80 18.00 18.20
3803.D 5080302.M Thu Mar 21 11:46:12 2002 Page 6 NYC-WTC_000037945
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NYC-WTC_000037945Source: NYC Law Department, mirrored locally
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