NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\031902\3803.D Vial: 13
Acq On : 19 Mar 2002 9:29 pm Operator: McLean
Sample : RE-INJ 2/20 Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
Peak Number 4 Trisiloxane, 1,1,1,5,5,5-he... Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
17.84 0.75 ug/L 353664 Ac enaphthene- dl 0 18.13
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H36O4Si5 003555-47-3 42
2 1,1,3,3,5,5,7,7,9,9,11,11-DODECA... 430 C12H38O5Si6 000000-00-0 40
3 Hexasiloxane, 1,1,3,3,5,5,7,7,9,... 430 C12H38O5Si6 000995-82-4 40
4 (trimethylsilyloxy) 2-(trimethy... 398 C18H27C104Si2 000000-00-0 28
Abundance Scan 1628 (17.843 min): 3803.D (-) m/z 73.10 100.00%
73
5000
147 281
327
T T 11
17.60 17.80 18.00 18.20
45
, 191 221 249.
m/z->
0-
—
50
117
• ■ i ■ Ir
100 150
' 1 1 f
200
1 1 1 1'1
250 300
Ll —383.415
350 400
m/z 147.10 37.35%
Abundance #322218: Trisiloxane. 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim...
73 147
281
5000 .A
'1 11'11’I
1 • • • • 1
17.60 17.80 18.00 18.20
m/z 281.00 35.41%
369
m/z—>
0 +
45
50
117
—1 1
100 150
207
177 |
Tfrr
200
249.
—
250
310 341
1 I 1 1 1 ‘ I •
400
300 350
[
1 1 I ' •
Abundance#347007: 1,1,3,3,5,5,77,9,9,11,11-DODECAMETHYL-HEXASILOXANE
73
• ■ i' ■ ‘ ‘ i .s.,.......
17.6017.80 18.0018.20
5000 m/z 327.00 11.81%
281
207
133
341 4=
m/z->
0- •45 — r
50 100
103
150 200
.253
1771123044
250
, 309, L 41
300 350 400
Abundance #347008: Hexasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11-dodecamethyl
73 1 • • ■ • 1 i • ■ • • 1
17.60 17.80 18.00 18.20
m/z 282.00 9.64%
5000
281
207
133
341
m/z—>
0 +
45 ।
50
-IP 1771—4 2302134 1 309 It
103
100 150 200 250 300
415
L
I ■ ■ • • l • ‘
350 400
1 • •'' i • ■ i • ■ • • i
17.60 17.80 18.00 18.20
3803.D 5080302.M Thu Mar 21 11:46:12 2002 Page 6
NYC-WTC_000037945
OCR can misread numbers and units. Confirm readings against the page image before using them.