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GCMS quantitative results for sample AE03799, March 22, 2002

Machine-extracted title · confidence 90%

Laboratory report listing concentrations of volatile organic compounds in sample AE03799 analyzed on March 22, 2002.

NYC-WTC_000037870–000037883

Folder label: “GCMS X 2/20/02 A 3/20/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031902\3799.D Vial: 9 Acq On : 19 Mar 2002 6:13 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 4 Trisiloxane, 1,1,1,5,5,5-he... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 17.84 1.08 ug/L 651240 Acenaphthene-dl0 18.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 59 2 Propanedioic acid, [(trimethylsi... 336 C12H28O5Si3 038165-93-4 38 3 Propanedioic acid, [(trimethylsi... 336 C12H28O5Si3 038165-93-4 38 4 3-Isopropoxy-l,1,1,7,7,7-hexamet... 576 C18H52O7Si7 071579-69-6 38 Abundance Scan 1628 (17.842 min): 3799.D (-) m/z 73.10 100.00% 73

5000 147 281 - 327 17.60 17.80 18.00 18.20 45

m/z-> 0- — 50 117 100 , 191 221 249 Ir TB FI — r 150 200 250 4383. 300 350 415 400 m/z 147.10 42.28%

Abundance #322218: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 73 147

281 5000- T T PAm 17.60 17.80 18.00 18.20 m/z 281.10 34.24% 369 45 207 249, 95117. 0- — r tT ri . — , 310 341 1 ....... 1744— m/z-> 50 100 150 200 250 300 350 400 Abundance #286009: Propanedioic acid, [(trimethylsilyl)oxy]-, bis(tr... 73 '11 ■11' f -PPP 17.6017.8018.0018.20 5000 m/z 327.00 14.78% 147 45 102 ___ I 1 177 221 265 222 321 0- I * TI r Tpt Pi 1rr i IT / । । । »'» । » । T — miz-> 50 100 150 200 250 300 350 400 Abundance #286008: Propanedioic acid, [(trimethylsilyl)oxy]-, bis(tr... 73 T ■ • • l T 17.60 17.80 18.00 18.20 m/z 282.10 9.11%

5000 147

45 102

0 —1+1 1 100 17 221 265 222 TFr ' I ' T 321 ' ' 1 1 1 1 ‘ I ' i ■ ’ • ' i • ■ T T I T T miz—> 50 150 200 250 300 350 400 17.60 17.80 18.00 18.20

3799.D 5080302.M Thu Mar 21 11:39:31 2002 Page 6

NYC-WTC_000037880

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