GCMS quantitative results for sample AE03799, March 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031902\3799.D Vial: 9 Acq On : 19 Mar 2002 6:13 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 3 Cyclohexasiloxane, dodecame... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

15.11 1.75 ug/L 967215 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 9 2 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6/* 4 3 5,6-exo-Epoxy-N-phenyl-l-trimeth... 341 C19H23NO3Si 000000-00/ /0 47 4 5-(2,3-BIS(TRIMETHYLSILYLOXY)PRO... 444 C20H40N205Si2 012774-3-8 25 Abundance Scan 1327 (15,112 min): 3799.D (-) m/ z 73.10. 100.00% 73

5000 341 T-r-p-TT-r-y-r 147 429 14.80 15.00 15.20 15.40 45 117 [ 179 207 251 311 [ - m/z 341.00 37.45% 0 I frti 11 — fr . 1* rl 1 ' ‘ 1 I miz-> 50 100 150 200 250 300 350 400 Abundance #352523: Cyclohexasiloxane, dodecamethyl- $$ Dodecamethylc... 73 341

429 5000 — 14.80 15.00 15.20 15.40 m/z 147.10 13.91% 147 45 117 L 207 t 267 311 397, 0- - TITT miz-> 50 100 150 200 250 300 350 400 Abundance #352522: Cyclohexasiloxane, dodecamethyl- 73 nmm 14.80 15.00 15.20 15.40 5000 m/z 429.10 13.35% 341 429 147 45 117 _1 _177' 207 237 271 3111 367 397 0- - 11 * TTTTTDTT miz-> 50 100 200 150 3 250 300 350 400 Abundance #290888: 5,6-exo-Epoxy-N-phenyl-1 -trimethylsilylmethylbicy... 73 -*PP 14.80 15.00 15.20 15.40 m/z 342.00 12.69%

5000, 326

0- ' ‘ I ' ‘ ‘ ' I ' ' ■ ' I ‘ ‘ • I ‘ ‘ I ' ' ‘ ‘ I ■ ‘ ' r I ' • ■ • I 1 1 m/z—> 50 100 150 200 250 300 350 400 14.80 15.00 15.20 15.40

3799.D 5080302.M Thu Mar 21 11:39:29 2002 Pace 5 NYC-WTC_000037879