Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03801 conducted on March 22, 2002.
NYC-WTC_000037906–000037926Folder label: “GCMS X 2/20/02 A 3/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
8 Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\031902\3801.D Vial; 11 Acq On ; 19 Mar 2002 7:51 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L
Peak Number 3 Cyclohexasiloxane, dodecame... Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
15.11 2.84 ug/L 1336120 Naphthalene-d8 13.03
Hit# of 5 Tentative ID MW MolForm CAS# Qual
l Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 91 2 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 91 3 5,6-exo-Epoxy-N-phenyl-l-trimeth... 341 C19H23NO3Si 000000-00-0 50 4 METHYL 2,3-BIS(TRIMETHYLSILYLOXY... 341 C16H27DO4Si2 000000-00-0 32 Abundance Scan 1327 (15.112 mln): 3801.D (-) m/z 73.10 100.00% 73
5000 341 -r-r-p-r-n-j-r ‘.................... f-m-i-p-m-f 147 429 45 14.80 15.00 15.20 15.40 io 207
n/z-> 0- — — r . I 179 । 251r4281 117 cs 3974 m/z 341.00 40.21% 100 150 200 250 300 350 400 Abundance exasiloxane, dodecamethyl-$$ Dodecamethylc... 73 341
5000 429 P 14.80 15.00 15.20 15.40 m/z 147.10 16.01% 147 45 0- 11 — ' , 117. ■ ■ ■ 207, . 267, . 311. i 397, m/z-> 50 100 ' ' 150 1200 250 300 350 400 Abundance me, dodecamethyl- 73 ----- 14.80 15.00 15.20 15.40 5000 m/z 429.10 14.28% 341 429 147 45 117 177 207 237 271 3111 367 397 0- I—f T T"TT0113 m/z-> Abundance 50 100 150 200 250 300 350 400 #290888: 5,6-exo-Epoxy-N-phenyl-1 -trimethylsilylmethylbicy... 73 T T k T 14.80 15.00 15.20 15.40 m/z 342.00 13.07% T
5000 326
miz—> 0 50 100 150 200 250 300 350 400 A 11 I 1 11'T 14.80 15.00 15.20 15.40
?A01 n EnRA00 M Thu Mar 21 11.A?.A4 onn2 Pace 5 NYC-WTC_000037915
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NYC-WTC_000037948
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03804 conducted on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037884
Instrument data file containing chromatographic scans and compound identification for environmental samples analyzed in March 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037870
Laboratory report listing concentrations of volatile organic compounds in sample AE03799 analyzed on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037964
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03805 conducted on March 22, 2002.
Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010610
Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012129
Laboratory report for GC/MS re-injection of sample 1639 using Method 508 scan on March 20-21, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010537
Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010659
Laboratory report detailing gas chromatography-mass spectrometry analysis of environmental sample AE02381 conducted on March 22, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010585
Laboratory analysis report for sample AE02338 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010488
Laboratory analysis report for sample AE02334 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010513
Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011347
Laboratory report documenting GCMS blank analysis of environmental sample AE03265 conducted on March 25, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000037819
Department of Environmental Protection site log sheet for the World Trade Center area covering February and March 2002.
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NYC-WTC_000037820
Log sheet recording sample preparation details including drip rates and pH for GCMS analysis in March 2002.
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NYC-WTC_000037825
Laboratory report listing quantitative concentrations of volatile organic compounds in sample AE00364 analyzed on March 21, 2002.
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NYC-WTC_000037829
Reference data report for GCMS analysis of sample AE00364 showing peak identification and response values from March 21, 2002.
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NYC-WTC_000037837
Laboratory report documenting GCMS analysis of a method blank for sample AE00364 to verify analytical system cleanliness.
Filed in the same folder