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GCMS analysis results for sample AE03804, March 22, 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03804 conducted on March 22, 2002.

NYC-WTC_000037948–000037963

Folder label: “GCMS X 2/20/02 A 3/20/02

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Scanned page image, NYC-WTC_000037957
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031902\3804.D Vial: 14 Acq On : 19 Mar 2002 10:18 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 3 Cyclohexasiloxane, dodecame... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 15.11 1.98 ug/L 818756 Naphthalene-d8 13.03 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Cyclohexasiloxane, dodecamethyl-... 444 C12H36O6Si6 000540-97-6 91 2 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 91 3 METHYL 2,3-BIS(TRIMETHYLSILYLOXY. .. 341 C16H27DO4Si2 000000-00-0 40 4 Silane, [1,2,3-benzenetriyltris(... 342 C15H30O3Si3 017864-23-2 22 Abundance Scan 1327 (15.112 min): 3804.D (-) m/z 73.10 100.00% 73

5000 341

147 v 1’111/1/1/1/1 ’ 11’1’111 ; * ‘ I 429 14.80 15.00 15.20 15.40 45 - 207 251 117 179 119- ao» 311 m/z 341.00 38.13 0- r T — 1 —f ■ m/z-> 50 100 150 200 250 300 350 ' ' 400 Abundance #352523: Cyclohexasiloxane, dodecamethyl- $$ Dodecamethylc... 73 341

429 — 5000 T T 1 14.80 15.00 15.20 15.40 m/z 147.10 15.76 147 45 117 207 267 311 397. 0- • • — 4 r "l • • • ■ i ■ • m/z—> 50 100 150 200 250 300 350 400 Abundance #352522: Cyd ' a > xane, dodecamethyl- 73 mPPP ,।y 14.80 15.00 15.20 15.40 5000 m/z 429.10 14.09 341 429 147 45 1 ) 117 I 177 207 237 271 3111 367 397 0 ‘ ‘I 1 TT .J.'..'. । I ■ T f 1T TTT TTP 1 T Pro *i TINT r ■ miz—> 50 100 150 200 250 300 350 400 Abundance#289709: METHYL 2,3-BIS(TRIMETHYLSlLYLOXY>-5-DEUTEROPHENf 73 180 14.80 15.00 15.20 15.40 m/z 342.00 13.93%

5000 341 45 ,106 .149 0- r — 1 . V TT 11 r .222 268 310.1 ......... mmmmm miz—> 50 100 150 200 250 300 ' 350 ' ‘ 400 14.80 15.00 15.20 15.40

3804.D 5080302.M Thu Mar 21 11:48:06 2002 Pace 5 NYC-WTC_000037957

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NYC-WTC_000037957Source: NYC Law Department, mirrored locally

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