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GCMS blank analysis results for sample AE03265, March 2002

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Laboratory report documenting GCMS blank analysis of environmental sample AE03265 conducted on March 25, 2002.

NYC-WTC_000011347–000011364

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\031902\0214LB.D Vial: 33 Acq On : 21 Mar 2002 5:58 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 3 Cyclohexasiloxane, dodecame... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

15.11 1.68 ug/L 1849620 Naphthalene-d8 13.04

Hit# of 5 Tentative ID MW MolForm CAS# Qual l Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 91 2 Cyclohexasiloxane, dodecamethyl- 444 C12H36O6Si6 000540-97-6 91 3 Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 23 4 Silane, [1,2,3-benzenetriyltris(... 342 C15H30O3Si3 017864-23-2 22 Abundance Scan 1327 (15.112 min): 0214LB.D (-) m/z 73.10 100.00% 73

5000

45 147 341

429 A 14.80 15.00 15.20 15.40 0- -4 . 117..1 . 179,2%7. .251 281 311 J, . . , 397,4 m/z 341.00 33.22% m/z-> 50 100 150 200 250 300 350* 400 Abundance #352523: Cyclohexasiloxane, dodecamethyl- $$ Dodecamethylc... 73 341

5000 429 ..... 1...... 14.80 15.00 15.20 15.40 m/z 147.10 13.89% 147

0- ri 45 3 . ..117.27 250 ‘ ' 300 350 ‘ ' 400 267 311 397 Tl/Z-> 50 100 150 200 Abundance #352522: Cyclohexasiloxane, dodecamethyl- 73 T T T T 14.80 15.00 15.20 15.40 5000 m/z 429.10 12.06% 341 429 147 45 0 - 117 .. .177.207.237 271 , 311, 367 397 •n/z-> 50 100 150 200 250 300 350 400 Abundance #352524: Cyclohexasiloxane, dodecamethyl- (CAS) $$ Dodecam... 73 341 ■' I ' ' " I ' ' * i * ■ ■ • i 429 14.80 15.00 15.20 15.40 m/z 342.00 11.28%

5000 147

207 0 /z—> 50 100 150 200 250 300 350 400 14.80 15.00 15.20 15.40

3214LB.D 5080302.M Mon Mar 25 08:59:18 2002 Page 5

NYC-WTC_000011356

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NYC-WTC_000011356Source: NYC Law Department, mirrored locally

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